S-phenyl 2-oxopropanethioate

Base Information

• Chemical Name: S-phenyl 2-oxopropanethioate
• CAS No.: 13884-99-6
• Molecular Formula: C9H8O2S
• Molecular Weight: 180.2236

Synonyms:

Chemical Property of S-phenyl 2-oxopropanethioate

Chemical Property:

• Vapor Pressure: 0.0323mmHg at 25°C
• Boiling Point: 243.3°C at 760 mmHg
• Flash Point: 95.5°C
• Density: 1.21g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of S-phenyl 2-oxopropanethioate

There total 6 articles about S-phenyl 2-oxopropanethioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

1,1-Dichloro-1-phenylsulfanyl-propan-2-one (137524-59-5) → α-keto S-phenyl thiopropanoate (13884-99-6)

Guidance literature:

With water; sodium hydrogencarbonate; In acetone; for 12h; Ambient temperature;

DOI:10.1080/00397919108019811

Reference yield: 10.0%

acetone (67-64-1) + diphenyldisulfane (882-33-7) → α-keto S-phenyl thiopropanoate (13884-99-6) + α,α-Bis(phenylthio)acetone (69753-44-2)

Guidance literature:

With potassium hydroxide; In tetrahydrofuran; for 6h; Ambient temperature;

DOI:10.1055/s-1980-29271

Reference yield:

1-phenylsulfanyl-1-(triphenylphosphoranylidene)-2-propanone (13884-96-3) → α-keto S-phenyl thiopropanoate (13884-99-6)

Guidance literature:

With lead(IV) acetate; In dichloromethane;

DOI:10.1007/BF00901458

upstream raw materials:

1-phenylsulfanyl-1-(triphenylphosphoranylidene)-2-propanone

1,1-Dichloro-1-phenylsulfanyl-propan-2-one

acetone

diphenyldisulfane

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