[(2-Methyl-2-phenylhydrazinecarbothioyl)sulfanyl]acetic acid

Base Information

Chemical Name:[(2-Methyl-2-phenylhydrazinecarbothioyl)sulfanyl]acetic acid
CAS No.:112768-84-0
Molecular Formula:C10H12N2O2S2
Molecular Weight:256.349
Hs Code.:
DSSTox Substance ID:DTXSID40548613
Wikidata:Q82427368

Synonyms:112768-84-0;DTXSID40548613;[(2-Methyl-2-phenylhydrazinecarbothioyl)sulfanyl]acetic acid

Suppliers and Price of [(2-Methyl-2-phenylhydrazinecarbothioyl)sulfanyl]acetic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of [(2-Methyl-2-phenylhydrazinecarbothioyl)sulfanyl]acetic acid

Chemical Property:

XLogP3:2.7
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:5
Exact Mass:256.03401998
Heavy Atom Count:16
Complexity:255

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN(C1=CC=CC=C1)NC(=S)SCC(=O)O

Technology Process of [(2-Methyl-2-phenylhydrazinecarbothioyl)sulfanyl]acetic acid

There total 1 articles about [(2-Methyl-2-phenylhydrazinecarbothioyl)sulfanyl]acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75-15-0,12122-00-8
carbon disulfide

: 3926-62-3
sodium monochloroacetic acid

: 618-40-6
1-Methyl-1-phenylhydrazine

: 112768-84-0
2-(3-Methyl-3-phenyl-thiocarbazoylthio)-essigsaeure

Guidance literature:: With triethylamine; Yield given. Multistep reaction; 1.) ether, 20 deg C, 1 h, 2.) water;
DOI:10.1002/ardp.19873200410

Reference yield: 58.0%

: 112768-84-0
2-(3-Methyl-3-phenyl-thiocarbazoylthio)-essigsaeure

: 112768-86-2
3-(N-Methyl-N-phenyl-amino)-2-thioxo-thiazolidin-4-on

Guidance literature:: With sulfuric acid; acetic anhydride; at 80 ℃; for 0.5h;
DOI:10.1002/ardp.19873200410

Reference yield:

: 112768-84-0
2-(3-Methyl-3-phenyl-thiocarbazoylthio)-essigsaeure

: 5-Benzyliden-3-(N-methyl-N-phenyl-amino)-2-thioxo-thiazolidin-4-on

Guidance literature:: Multi-step reaction with 2 steps

1: 58 percent / acetic anhydride, H₂SO₄ / 0.5 h / 80 °C

2: 95 percent / piperidine / ethanol / 0.5 h / Heating

With piperidine; sulfuric acid; acetic anhydride; In ethanol;
DOI:10.1002/ardp.19873200410