Benzenepropanethioamide, b-oxo-N-2-pyridinyl-

Base Information

• Chemical Name: Benzenepropanethioamide, b-oxo-N-2-pyridinyl-
• CAS No.: 113576-62-8
• Molecular Formula: C14H12N2OS
• Molecular Weight: 256.328
• Mol file: 113576-62-8.mol

Synonyms:

Chemical Property of Benzenepropanethioamide, b-oxo-N-2-pyridinyl-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Benzenepropanethioamide, b-oxo-N-2-pyridinyl-

There total 2 articles about Benzenepropanethioamide, b-oxo-N-2-pyridinyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

pyridin-2-yl-dithiocarbamic acid methyl ester (13037-46-2) → N-(2'-pyridinyl)benzoylthioacetamide (113576-62-8)

Guidance literature:

Multi-step reaction with 2 steps

1: xylene / 3 h / Heating

2: 2.) 10 percent potassium hydroxide, carbon dioxide / 1.) xylene, 3 d; 2.) water, 3 h, room temperature

With potassium hydroxide; carbon dioxide; In xylene;

Reference yield:

2-pyridylisothiocyanate (52648-45-0) + sodium dibenzoylmethane (19269-14-8) → N-(2'-pyridinyl)benzoylthioacetamide (113576-62-8)

Guidance literature:

With potassium hydroxide; carbon dioxide; Yield given. Multistep reaction; 1.) xylene, 3 d; 2.) water, 3 h, room temperature;

Reference yield: 67.0%

copper(II) acetate monohydrate (6046-93-1) + N-(2'-pyridinyl)benzoylthioacetamide (113576-62-8) → {Cu(N-(2-pyridinyl)benzoylthioacetamide(-))2}

Guidance literature:

In acetone; cooled for 5 h in an acetone-dry ice bath, bubbled N2 into the reaction mixture; filtration pf pptn., dried in air and then in vac. over P2O5; elem. anal.;

upstream raw materials:

2-pyridylisothiocyanate

sodium dibenzoylmethane

pyridin-2-yl-dithiocarbamic acid methyl ester

Downstream raw materials:

N-benzyl-N-(2-pyridinyl)benzoylthioacetamide

2-benzoylmethylidene-2H-pyrido<2,3-a><1,2,4>thiadiazole