2-Ethoxyphenylcarbamic acid methyl ester

Base Information

Chemical Name:2-Ethoxyphenylcarbamic acid methyl ester
CAS No.:113932-79-9
Molecular Formula:C10H13NO3
Molecular Weight:195.218
Hs Code.:
DSSTox Substance ID:DTXSID60876046
Nikkaji Number:J1.558.790C
Wikidata:Q82857559
Mol file:113932-79-9.mol

Synonyms:113932-79-9;SCHEMBL10895253;DTXSID60876046;AKOS003799246;2-Ethoxyphenylcarbamic acid methyl ester;Carbamic acid, (2-ethoxyphenyl)-, methyl ester

Suppliers and Price of 2-Ethoxyphenylcarbamic acid methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Ethoxyphenylcarbamic acid methyl ester

Chemical Property:

XLogP3:2.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:195.08954328
Heavy Atom Count:14
Complexity:184

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCOC1=CC=CC=C1NC(=O)OC

Technology Process of 2-Ethoxyphenylcarbamic acid methyl ester

There total 2 articles about 2-Ethoxyphenylcarbamic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 67-56-1
methanol

: 938-73-8
2-ethoxybenzamide

: 113932-79-9
methyl 2-ethoxyphenylcarbamate

Guidance literature:: With 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; silver(I) acetate; In N,N-dimethyl-formamide; for 12h; Ambient temperature; or NBS-Hg(OAc)2;
DOI:10.1016/0040-4039(90)80016-F

Reference yield:

: 134-11-2
2-ethoxybenzoic acid

: 113932-79-9
methyl 2-ethoxyphenylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride; N,N-dimethyl-formamide / 24 h / 20 °C

2: ammonium hydroxide / chloroform / -10 °C

3: lithium hydroxide monohydrate; N-bromoacetamide / 24 h / 0 - 25 °C / Darkness

With ammonium hydroxide; thionyl chloride; lithium hydroxide monohydrate; N,N-dimethyl-formamide; N-bromoacetamide; In chloroform; 3: |Hofmann Rearrangement;
DOI:10.1055/s-0035-1561405