2,4,6,8,10,12-Hexaoxatridecane

Base Information

• Chemical Name: 2,4,6,8,10,12-Hexaoxatridecane
• CAS No.: 13352-76-6
• Molecular Formula: C7H16O6
• Molecular Weight: 196.2
• Mol file: 13352-76-6.mol

Synonyms:1,9-dimethoxy-2,4,6,8-tetraoxa-nonane;CH3-(OCH2)5-OCH3;bis-(methoxymethoxy-methoxy)-methane;2,4,6,8,10,12-Hexaoxatridecane;

Chemical Property of 2,4,6,8,10,12-Hexaoxatridecane

Chemical Property:

• Melting Point: 18.3 °C
• Boiling Point: 123-135℃/8Torr
• PSA: 55.38000
• Density: 1.1003 g/cm3(Temp: 25 °C)
• LogP: 0.13310
• Storage Temp.: 2-8°C

Purity/Quality:

98%Min ^*data from raw suppliers

2,4,6,8,10,12-Hexaoxatridecane 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,4,6,8,10,12-Hexaoxatridecane

There total 12 articles about 2,4,6,8,10,12-Hexaoxatridecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ POMM5 (13352-76-6)

Guidance literature:

Methylal, Trioxan unter Zusatz von H2SO4 (5-stdg. Kohen);

Reference yield:

1,3,5-Trioxan (110-88-3) + 1,1-dimethoxyethane (534-15-6) → C11H24O10 + C13H28O12 + bis-methoxymethoxy-methane (13353-03-2) + bis(methoxymethyl)ether (628-90-0) + POMM4 (13352-75-5) + CH3-(OCH2)8-OCH3 (13352-78-8) + Methoxymethoxymethoxymethoxymethoxy-methoxymethoxymethoxymethoxymethoxymethoxy-methane (54261-86-8) + POMM5 (13352-76-6) + CH3-(OCH2)7-OCH3 (13353-04-3) + CH3-(OCH2)6-OCH3 (13352-77-7)

Guidance literature:

Amberlite IR 120; at 100 ℃; for 24h; Product distribution / selectivity;

Reference yield:

1,3,5-Trioxan (110-88-3) + 1,1-dimethoxyethane (534-15-6) + bis(methoxymethyl)ether (628-90-0) → C11H24O10 + C13H28O12 + bis-methoxymethoxy-methane (13353-03-2) + POMM4 (13352-75-5) + CH3-(OCH2)8-OCH3 (13352-78-8) + Methoxymethoxymethoxymethoxymethoxy-methoxymethoxymethoxymethoxymethoxymethoxy-methane (54261-86-8) + POMM5 (13352-76-6) + CH3-(OCH2)7-OCH3 (13353-04-3) + CH3-(OCH2)6-OCH3 (13352-77-7)

Guidance literature:

sulfuric acid; In water; at 100 ℃; for 12h; Product distribution / selectivity;

upstream raw materials:

1,3,5-Trioxan

1,1-dimethoxyethane

bis(methoxymethyl)ether

formaldehyd

Downstream raw materials:

Bis(2-hydroxyphenyl)methane

2-[(4-hydroxyphenyl)methyl]phenol

bis-(4-hydroxyphenyl)methane

Refernces

• 1、 Peter, Andreas,Fehr, Samuel M.,Dybbert, Valentin,Himmel, Daniel,Lindner, Ines,Jacob, Eberhard,Ouda, Mohamed,Schaadt, Achim,White, Robin J.,Scherer, Harald,Krossing, Ingo. "Towards a Sustainable Synthesis of Oxymethylene Dimethyl Ether by Homogeneous Catalysis and Uptake of Molecular Formaldehyde". supporting information. p. 9461 - 9464. Retrieved 2018/07/25.
• 2、 -. "REACTION SYSTEM AND PROCESS FOR PREPARING POLYMETHOXY DIMETHYL ETHER". Paragraph 0105-0108. . Retrieved 2015/04/15.