4-(1,3,6,2-Dioxazaborocan-2-yl)benzaldehyde

Base Information

Chemical Name:4-(1,3,6,2-Dioxazaborocan-2-yl)benzaldehyde
CAS No.:128399-19-9
Molecular Formula:C11H14BNO3
Molecular Weight:219.048
Hs Code.:
DSSTox Substance ID:DTXSID50560644
Nikkaji Number:J2.836.634E
Wikidata:Q82444115

Synonyms:4-(1,3,6,2-Dioxazaborocan-2-yl)benzaldehyde;128399-19-9;DTXSID50560644

Suppliers and Price of 4-(1,3,6,2-Dioxazaborocan-2-yl)benzaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 4-(1,3,6,2-Dioxazaborocan-2-yl)benzaldehyde

Chemical Property:

Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:219.1066735
Heavy Atom Count:16
Complexity:211

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:B1(OCCNCCO1)C2=CC=C(C=C2)C=O

Technology Process of 4-(1,3,6,2-Dioxazaborocan-2-yl)benzaldehyde

There total 1 articles about 4-(1,3,6,2-Dioxazaborocan-2-yl)benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 87199-17-5
4-formylphenylboronic acid,

: 111-42-2
2,2'-iminobis[ethanol]

: 128399-19-9
4-formylphenyl boronic acid diethanolamine ester

Guidance literature:: In tetrahydrofuran; isopropyl alcohol; to soln. of 4-formylphenylboronic acid (6.7 mmol) in THF soln. of diethanolamine (7.3 mmol) in 2-propanol added, stirred for 3h at room temp.; filtered, washed with THF, dried;
DOI:10.1016/j.jorganchem.2010.09.002

Reference yield:

: 128399-19-9
4-formylphenyl boronic acid diethanolamine ester

: 74-89-5
methylamine

: C₁₂H₁₉BN₂O₂

Guidance literature:: 4-formylphenyl boronic acid diethanolamine ester; methylamine; In methanol; at 20 ℃;

With hydrogenchloride; methanol; sodium tetrahydroborate; at 30 ℃; for 2h; pH=4 - 6;