Technology Process of mercury bromide iodide
There total 5 articles about mercury bromide iodide which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
dichloromethane;
byproducts: CH3COCH3; addn. of aq. HI (0.002mole; 56%) to a mixture of α-OH-ferrocenylalkylate (0.002mole) and Hg compd. (0.002mole) in CH2Cl2 (5ml) with stirring; stirring, 2-3h, 23.+-.0.5°C;; addn. of (C2H5)2O; filtration; washing ppt. with Et2O/CH2Cl2 (2:1); washing filtrate with H2O, drying with Na2SO4; removal of solvent in vac. (not above 30°C); dissolving in C6H6/ether (1:2); chromy.; evapn., room temp.; recrystn.; elem. anal.;;
- Guidance literature:
-
In
dichloromethane;
byproducts: C6H6; addn. of aq. HI (0.002mole; 56%) to a mixture of α-OH-ferrocenylalkylate (0.002mole) and Hg compd. (0.002mole) in CH2Cl2 (5ml) with stirring; stirring, 2-3h, 23.+-.0.5°C;; addn. of (C2H5)2O; filtration; washing ppt. with Et2O/CH2Cl2 (2:1); washing filtrate with H2O, drying with Na2SO4; removal of solvent in vac. (not above 30°C); dissolving in C6H6/ether (1:2); chromy.; evapn., room temp.; recrystn.; elem. anal.;;
- Guidance literature:
-
In
dichloromethane;
byproducts: C6H6; addn. of aq. HI (0.002mole; 56%) to a mixture of C5H5FeC5H4CH(CH3)OH (0.002mole) and Hg compd. (0.002mole) in CH2Cl2 (5ml) with stirring; stirring, 2-3h, 23.+-.0.5°C;; addn. of (C2H5)2O; filtration; washing ppt. with Et2O/CH2Cl2 (2:1); washing filtrate with H2O, drying with Na2SO4; removal of solvent in vac. (not above 30°C); dissolving in C6H6/ether (1:2); chromy.; evapn., room temp.; recrystn.; elem. anal.;;
