4,7-Dithia-1,10-diphosphadecane, 1,1,10,10-tetraphenyl-

Base Information

Chemical Name:4,7-Dithia-1,10-diphosphadecane, 1,1,10,10-tetraphenyl-
CAS No.:15610-21-6
Molecular Formula:C30H32P2S2
Molecular Weight:518.664
Hs Code.:
DSSTox Substance ID:DTXSID50477344
Nikkaji Number:J1.232.562B
Wikidata:Q82309792
Mol file:15610-21-6.mol

Synonyms:15610-21-6;DTXSID50477344;4,7-Dithia-1,10-diphosphadecane, 1,1,10,10-tetraphenyl-

Suppliers and Price of 4,7-Dithia-1,10-diphosphadecane, 1,1,10,10-tetraphenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 4,7-Dithia-1,10-diphosphadecane, 1,1,10,10-tetraphenyl-

Chemical Property:

XLogP3:7.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:13
Exact Mass:518.14206736
Heavy Atom Count:34
Complexity:424

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)P(CCSCCSCCP(C2=CC=CC=C2)C3=CC=CC=C3)C4=CC=CC=C4

Technology Process of 4,7-Dithia-1,10-diphosphadecane, 1,1,10,10-tetraphenyl-

There total 1 articles about 4,7-Dithia-1,10-diphosphadecane, 1,1,10,10-tetraphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 420-12-2
thirane

: 106-93-4
ethylene dibromide

: 829-85-6
diphenylphosphane

: 15610-21-6
bis(diphenylphosphinodiethylene)ethylenedisulfide

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction; 1.) THF, hexane, -78 deg C, 2 h; 2.) THF, hexane, overnight;
DOI:10.1039/DT9960001261

Reference yield: 90.0%

: 60969-19-9
thallium(I) hexafluorophosphate

: 15610-21-6
bis(diphenylphosphinodiethylene)ethylenedisulfide

: palladium dichloride

: Pd((CH₂SCH₂CH₂P(C₆H₅)2)2)⁽²⁺⁾*2PF₆^(1-)=[Pd((CH₂SCH₂CH₂P(C₆H₅)2)2)](PF₆)2

Guidance literature:: In acetonitrile; byproducts: TlCl; stoich. amts., refluxing under N2 for 3 h; cooling, filtration off of TlCl, vol. reduction (vac.), pptn. on Et2O addn., recrystn. (CH2Cl2/Et2O); elem. anal.;