5-(Furan-2-yl)furan-2-carbaldehyde

Base Information

• Chemical Name: 5-(Furan-2-yl)furan-2-carbaldehyde
• CAS No.: 16303-60-9
• Molecular Formula: C9H6O3
• Molecular Weight: 162.145
• DSSTox Substance ID: DTXSID301303907
• Nikkaji Number: J1.908.763H
• Mol file: 16303-60-9.mol

Synonyms:5-(furan-2-yl)furan-2-carbaldehyde;16303-60-9;[2,2'-bifuran]-5-carbaldehyde;SCHEMBL9045232;FAGYPMBOOVLXAO-UHFFFAOYSA-N;DTXSID301303907;[2,2'-Bifuran]-5-carboxaldehyde;AKOS004118638;BS-48197;EN300-239531;F73827;F2167-0882

Chemical Property of 5-(Furan-2-yl)furan-2-carbaldehyde

Chemical Property:

• XLogP3: 1.5
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 2
• Exact Mass: 162.031694049
• Heavy Atom Count: 12
• Complexity: 169

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1=COC(=C1)C2=CC=C(O2)C=O

Technology Process of 5-(Furan-2-yl)furan-2-carbaldehyde

There total 3 articles about 5-(Furan-2-yl)furan-2-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,2'-bifuran (5905-00-0) → [2,2']bifuranyl-5-carbaldehyde (16303-60-9)

Guidance literature:

With hydrogenchloride; diethyl ether; hydrogen cyanide; anschliessendes Behandeln mit Wasser;

DOI:10.1002/hlca.193201501116

Reference yield:

ethyl 3-(2-furyl)-3-oxopropanoate (615-09-8) → [2,2']bifuranyl-5-carbaldehyde (16303-60-9)

Guidance literature:

Multi-step reaction with 3 steps

1: aq. NaOH solution / Erwaermen der bei 86-98/0.5 Torr siedenden Anteile des Reaktionsprodukts mit wss.-aethanol. Kalilauge

2: quinoline; copper oxide-chromium oxide / 200 °C

3: hydrogen cyanide; diethyl ether; hydrogen chloride / anschliessendes Behandeln mit Wasser

With quinoline; hydrogenchloride; sodium hydroxide; diethyl ether; hydrogen cyanide; copper oxide-chromium oxide;

DOI:10.1002/hlca.193201501116

Reference yield:

hydrogenchloride (7647-01-0,15364-23-5) + 2,2'-bifuran (5905-00-0) + diethyl ether (60-29-7,927820-24-4) + hydrogen cyanide (74-90-8) → [2,2']bifuranyl-5-carbaldehyde (16303-60-9)

Guidance literature:

Anschliessendes Behandeln mit Wasser;

DOI:10.1002/hlca.193201501116

upstream raw materials:

2,2'-bifuran

hydrogenchloride

diethyl ether

hydrogen cyanide

Downstream raw materials:

[2,2']bifuryl-5-carboxylic acid