2-Chloro-4-(chloromethyl)-1-(1-methylethoxy)benzene

Base Information

• Chemical Name: 2-Chloro-4-(chloromethyl)-1-(1-methylethoxy)benzene
• CAS No.: 32695-20-8
• Molecular Formula: C10H12 Cl2 O
• Molecular Weight: 219.111
• European Community (EC) Number: 251-162-6
• DSSTox Substance ID: DTXSID70186360
• Nikkaji Number: J319.421C
• Wikidata: Q83057630
• Mol file: 32695-20-8.mol

Synonyms:32695-20-8;2-Chloro-4-(chloromethyl)-1-(1-methylethoxy)benzene;EINECS 251-162-6;SCHEMBL10088641;DTXSID70186360;AKOS010948953

Chemical Property of 2-Chloro-4-(chloromethyl)-1-(1-methylethoxy)benzene

Chemical Property:

• Vapor Pressure: 0.00442mmHg at 25°C
• Boiling Point: 286.9°Cat760mmHg
• Flash Point: 80.9°C
• PSA: 9.23000
• Density: 1.175g/cm³
• LogP: 3.86600
• XLogP3: 3.6
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 3
• Exact Mass: 218.0265204
• Heavy Atom Count: 13
• Complexity: 150

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(C)OC1=C(C=C(C=C1)CCl)Cl

Technology Process of 2-Chloro-4-(chloromethyl)-1-(1-methylethoxy)benzene

There total 3 articles about 2-Chloro-4-(chloromethyl)-1-(1-methylethoxy)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-monochlorophenol (95-57-8) → 2-chloro-4-(chloromethyl)-1-(1-methylethoxy)benzene (32695-20-8)

Guidance literature:

Multi-step reaction with 2 steps

1: NaOEt

2: HCl, As₂O₃

With hydrogenchloride; sodium ethanolate; arsenic(III) trioxide;

DOI:10.1135/cccc19771723

Reference yield:

formaldehyd (50-00-0,30525-89-4,61233-19-0) + 1-chloro-2-(1-methylethoxy)benzene (42489-57-6) → 2-chloro-4-(chloromethyl)-1-(1-methylethoxy)benzene (32695-20-8)

Guidance literature:

With hydrogenchloride; arsenic(III) trioxide;

DOI:10.1135/cccc19771723

Reference yield:

→ 2-chloro-4-(chloromethyl)-1-(1-methylethoxy)benzene (32695-20-8)

Guidance literature:

2-Isopropoxy-chlorbenzol/Formalin/HCl in Eisessig;

upstream raw materials:

formaldehyd

1-chloro-2-(1-methylethoxy)benzene

2-monochlorophenol

Downstream raw materials:

[4-(3-Chloro-4-isopropoxy-benzyloxy)-phenyl]-acetic acid

3-chloro-4-(3'-chloro-4'-isopropoxybenzyloxy) phenylacetic acid

[4-(3-Chloro-4-isopropoxy-benzyloxy)-3-methyl-phenyl]-acetic acid

2-[3-Chloro-4-(3-chloro-4-isopropoxy-benzyloxy)-phenyl]-propionic acid

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