[2,4,6-Tri(propan-2-yl)phenyl]germane

Base Information

Chemical Name:[2,4,6-Tri(propan-2-yl)phenyl]germane
CAS No.:190080-49-0
Molecular Formula:C₁₅H₂₆Ge
Molecular Weight:278.961
Hs Code.:
DSSTox Substance ID:DTXSID10773697
Mol file:190080-49-0.mol

Synonyms:[2,4,6-Tri(propan-2-yl)phenyl]germane;190080-49-0;DTXSID10773697

Suppliers and Price of [2,4,6-Tri(propan-2-yl)phenyl]germane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of [2,4,6-Tri(propan-2-yl)phenyl]germane

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:3
Exact Mass:277.1011535
Heavy Atom Count:16
Complexity:190

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(C)C1=CC(=C(C(=C1)C(C)C)[Ge])C(C)C

Technology Process of [2,4,6-Tri(propan-2-yl)phenyl]germane

There total 1 articles about [2,4,6-Tri(propan-2-yl)phenyl]germane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 16853-85-3
lithium aluminium tetrahydride

: 10038-98-9
germaniumtetrachloride

: 108894-99-1
(2,4,6-triisopropylphenyl)magnesium bromide

: 190080-49-0
2,4,6-triisopropylphenylgermane

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; diethyl ether; byproducts: (CH3CHCH3)3C6H3; high vac. techniques; addn. of soln. of IsMgBr in THF to soln. of GeCl4 in Et2O (0°C), refluxing 1 h, addn. of HCl (10 %), phase separation, distillation, dissoln. in Et2O and addn. into suspn. of LiAlH4 in Et2O, refluxing 2 h, hydrolysing; drying (over Na2SO4), distillation; further intermediate: (CH3CHCH3)3C6H2GeCl3;
DOI:10.1080/00945719708000207

Reference yield: 76.0%

: 56-23-5
tetrachloromethane

: 190080-49-0
2,4,6-triisopropylphenylgermane

: 190080-50-3
trichloro(2,4,6-triisopropylphenyl)germane

Guidance literature:: With α,α'-azo-bis-isobutyronitril; In tetrachloromethane; benzene; high vac. techniques; addn. of soln. of Ge compound in C6H6 to suspn. ofAIBN in CCl4, refluxing (1 h); solvent removal (vac.), recrystn. (pentane); elem. anal.;
DOI:10.1080/00945719708000207

Reference yield: 71.0%

: 128-09-6
N-chloro-succinimide

: 190080-49-0
2,4,6-triisopropylphenylgermane

: 190080-51-4
chloro(2,4,6-triisopropylphenyl)germane

Guidance literature:: In tetrahydrofuran; high vac. techniques; addn. of N-chlorosuccinimide to soln. of Ge compound, refluxing (1 h); solvent removal, addn. of pentane, filtration, crystn.; elem. anal.;
DOI:10.1080/00945719708000207