3,4-Dichlorotetrahydrofuran

Base Information

• Chemical Name: 3,4-Dichlorotetrahydrofuran
• CAS No.: 35128-44-0
• Molecular Formula: C4H6Cl2O
• Molecular Weight: 140.997
• NSC Number: 81209
• DSSTox Substance ID: DTXSID20292263
• Mol file: 35128-44-0.mol

Synonyms:3,4-Dichlorotetrahydrofuran;35128-44-0;NSC81209;SCHEMBL7703609;DTXSID20292263;CCG-40421;NSC-81209

Chemical Property of 3,4-Dichlorotetrahydrofuran

Chemical Property:

• Vapor Pressure: 0.251mmHg at 25°C
• Boiling Point: 212.5°Cat760mmHg
• Flash Point: 161.6°C
• Density: 1.32g/cm³
• XLogP3: 1.2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 0
• Exact Mass: 139.9795702
• Heavy Atom Count: 7
• Complexity: 58.7

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1C(C(CO1)Cl)Cl

Technology Process of 3,4-Dichlorotetrahydrofuran

There total 3 articles about 3,4-Dichlorotetrahydrofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,5-dihydrofuran (1708-29-8) → furan (110-00-9) + 2,3-dichlorotetrahydrofuran (3511-19-1) + 3,4-dichlorotetrahydrofuran (35128-44-0) + 3-hydroxydihydro-2(3H)-furanone + tetrahydropyran-4-enyl chloride (24265-21-2) + 2,3-Dichloro-1-propanol (616-23-9) + 2-buten-4-olide (497-23-4)

Guidance literature:

With clorine; at 24.84 ℃; under 800 Torr; Kinetics; Inert atmosphere; Gas phase;

DOI:10.1002/kin.20765

Reference yield:

2,5-dihydrofuran (1708-29-8) → 3,4-dichlorotetrahydrofuran (35128-44-0)

Guidance literature:

With tetrachloromethane; chlorine;

Reference yield:

→ (3S,4R)-3,4-Dichloro-tetrahydro-furan (19319-21-2,35128-44-0)

Guidance literature:

aus Verb. 2, Na-methanolat;

upstream raw materials:

2,5-dihydrofuran

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