Dodecanoic acid, 12,12-dimethoxy-, methyl ester

Base Information

Chemical Name:Dodecanoic acid, 12,12-dimethoxy-, methyl ester
CAS No.:1931-67-5
Molecular Formula:C15H30O4
Molecular Weight:274.401
Hs Code.:
Mol file:1931-67-5.mol

Synonyms:methyl 12,12-dimethoxydodecanoate;12-Oxododecansaeuremethylesterdimethylacetal;Methyl-11-formylundecanoat-acetal;12.12-Dimethoxydodecanoate;

Suppliers and Price of Dodecanoic acid, 12,12-dimethoxy-, methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Dodecanoic acid, 12,12-dimethoxy-, methyl ester

Chemical Property:

PSA：44.76000
LogP:3.67930

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Dodecanoic acid, 12,12-dimethoxy-, methyl ester

There total 1 articles about Dodecanoic acid, 12,12-dimethoxy-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 67-56-1
methanol

: 69381-33-5
α-iodocyclododecanone

: 1931-67-5
12,12-dimethoxydodecanoic acid methyl ester

: 42858-38-8
(E)/(Z)-cyclododec-2-enone

: 76331-08-3
2-methoxycyclododecanone

: 830-13-7
cyclododecanone

Guidance literature:: at 20 ℃; for 480h; Further byproducts given; Photolysis;
DOI:10.1246/bcsj.73.1645

Reference yield: 68.0%

: 122-97-4
3-Phenyl-1-propanol

: 1931-67-5
12,12-dimethoxydodecanoic acid methyl ester

: methyl 12-methoxy-12-(3-phenylpropoxy)dodecanoate

Guidance literature:: 12,12-dimethoxydodecanoic acid methyl ester; With 2,4,6-trimethyl-pyridine; trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 0 ℃; Inert atmosphere;

3-Phenyl-1-propanol; In dichloromethane; at 0 ℃; Inert atmosphere;
DOI:10.1021/acs.joc.8b00675

Reference yield:

: 122-97-4
3-Phenyl-1-propanol

: 1931-67-5
12,12-dimethoxydodecanoic acid methyl ester

: methyl 12-(3-phenylpropoxy)dodecanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 2,4,6-trimethyl-pyridine; trimethylsilyl trifluoromethanesulfonate / dichloromethane / 0 °C / Inert atmosphere

1.2: 0 °C / Inert atmosphere

2.1: 2,4,6-trimethyl-pyridine; trimethylsilyl trifluoromethanesulfonate / dichloromethane / -30 °C / Inert atmosphere

2.2: -30 - 0 °C / Inert atmosphere

With 2,4,6-trimethyl-pyridine; trimethylsilyl trifluoromethanesulfonate; In dichloromethane;
DOI:10.1021/acs.joc.8b00675