Technology Process of Dodecanoic acid, 12,12-dimethoxy-, methyl ester
There total 1 articles about Dodecanoic acid, 12,12-dimethoxy-, methyl ester which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
at 20 ℃;
for 480h;
Further byproducts given;
Photolysis;
DOI:10.1246/bcsj.73.1645
- Guidance literature:
-
12,12-dimethoxydodecanoic acid methyl ester;
With
2,4,6-trimethyl-pyridine; trimethylsilyl trifluoromethanesulfonate;
In
dichloromethane;
at 0 ℃;
Inert atmosphere;
3-Phenyl-1-propanol;
In
dichloromethane;
at 0 ℃;
Inert atmosphere;
DOI:10.1021/acs.joc.8b00675
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: 2,4,6-trimethyl-pyridine; trimethylsilyl trifluoromethanesulfonate / dichloromethane / 0 °C / Inert atmosphere
1.2: 0 °C / Inert atmosphere
2.1: 2,4,6-trimethyl-pyridine; trimethylsilyl trifluoromethanesulfonate / dichloromethane / -30 °C / Inert atmosphere
2.2: -30 - 0 °C / Inert atmosphere
With
2,4,6-trimethyl-pyridine; trimethylsilyl trifluoromethanesulfonate;
In
dichloromethane;
DOI:10.1021/acs.joc.8b00675