N-BENZYL-N-ETHYLMETHYLAMINE

Base Information

• Chemical Name: N-BENZYL-N-ETHYLMETHYLAMINE
• CAS No.: 4788-37-8
• Molecular Formula: C10H15 N
• Molecular Weight: 149.236
• Hs Code.: 2921499090
• Mol file: 4788-37-8.mol

Synonyms:Benzylamine,N-ethyl-N-methyl- (7CI,8CI); N-Ethyl-N-methylbenzenemethanamine;N-Ethyl-N-methylbenzylamine; NSC 66252

Chemical Property of N-BENZYL-N-ETHYLMETHYLAMINE

Chemical Property:

• Vapor Pressure: 0.645mmHg at 25°C
• Refractive Index: 1.4995
• Boiling Point: 187°Cat760mmHg
• Flash Point: 59.4°C
• PSA: 3.24000
• Density: 0.918g/cm³
• LogP: 2.13830

Purity/Quality:

98% ^*data from raw suppliers

N-Ethyl-N-methylbenzylamine ^*data from reagent suppliers

Safty Information:

• Pictogram(s): R34:Causes burns.
• Hazard Codes: R34:Causes burns.
• Statements: 34
• Safety Statements: 26-36/37/39-45

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-BENZYL-N-ETHYLMETHYLAMINE

There total 12 articles about N-BENZYL-N-ETHYLMETHYLAMINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

ethyl iodide (75-03-6) + benzyl-methyl-amine (103-67-3) → N-ethyl-N-methylbenzylamine (4788-37-8)

Guidance literature:

With di-isopropyl azodicarboxylate; polymer-bound triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 12h;

DOI:10.1016/j.tetlet.2006.05.038

Reference yield: 82.0%

N-(Benzotriazol-1-yl-phenyl-methyl)-N-methyl-acetamide (147227-64-3) → N-ethyl-N-methylbenzylamine (4788-37-8)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; for 15h; Heating;

DOI:10.1021/jo00060a025

Reference yield: 76.0%

→ N-ethyl-N-methylbenzylamine (4788-37-8)

Guidance literature:

With triethyl borane; phenylsilane; sodium hydroxide; In tetrahydrofuran; tert-butyl methyl ether; at 20 ℃; for 48h; Sealed tube;

With hydrogenchloride; In tetrahydrofuran; tert-butyl methyl ether; water; at 20 ℃; for 6h;

upstream raw materials:

formic acid

N-ethylbenzylamine

N-Ethylmethylamine

benzyl chloride

Downstream raw materials:

N-Ethylmethylamine

9,10-dihydro-10-methylacridine

10-methyl-9, 10-dihydro-9-acridinone

N-ethylbenzylamine