4-Pentynoic acid, 2-[[(1,1-dimethylethoxy)carbonyl]amino]-, methyl ester, (2R)-

Base Information Edit

Chemical Name:4-Pentynoic acid, 2-[[(1,1-dimethylethoxy)carbonyl]amino]-, methyl ester, (2R)-
CAS No.:208709-76-6
Molecular Formula:C11H17NO4
Molecular Weight:227.26
Hs Code.:
Mol file:208709-76-6.mol

Synonyms:

Suppliers and Price of 4-Pentynoic acid, 2-[[(1,1-dimethylethoxy)carbonyl]amino]-, methyl ester, (2R)-

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 4-Pentynoic acid, 2-[[(1,1-dimethylethoxy)carbonyl]amino]-, methyl ester, (2R)- Edit

Chemical Property:

Purity/Quality:: 98.5% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4-Pentynoic acid, 2-[[(1,1-dimethylethoxy)carbonyl]amino]-, methyl ester, (2R)-

There total 12 articles about 4-Pentynoic acid, 2-[[(1,1-dimethylethoxy)carbonyl]amino]-, methyl ester, (2R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 67-56-1
methanol

: 24424-99-5
di-tert-butyl dicarbonate

: 23235-01-0,23235-03-2,50428-03-0,64165-64-6
(R)-2-aminopent-4-ynoic acid

: 208709-76-6,173306-82-6
(R)-N-Boc-propargylglycine methyl ester

Guidance literature:: methanol; (R)-2-aminopent-4-ynoic acid; With thionyl chloride; at 0 - 20 ℃;

di-tert-butyl dicarbonate; With sodium hydrogencarbonate; In 1,4-dioxane; at 20 ℃; Saturated solution;

Reference yield: 95.0%

: 74-88-4
methyl iodide

: 208709-76-6,173306-82-6
(R)-N-Boc-propargylglycine methyl ester

Guidance literature:: (R)-2-((tert-butoxycarbonyl)amino)pent-4-ynoic acid; With caesium carbonate; In DMF (N,N-dimethyl-formamide); at 20 ℃; for 0.75h;

methyl iodide; In DMF (N,N-dimethyl-formamide); for 3h;

With water; In DMF (N,N-dimethyl-formamide);

Reference yield: 95.0%

: 61172-66-5,63039-48-5,143979-37-7,63039-46-3
(R)-2-((tert-butoxycarbonyl)amino)pent-4-ynoic acid

: 74-88-4
methyl iodide

: 208709-76-6,173306-82-6
(R)-N-Boc-propargylglycine methyl ester

Guidance literature:: (R)-2-((tert-butoxycarbonyl)amino)pent-4-ynoic acid; With caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 0.75h;

methyl iodide; In N,N-dimethyl-formamide; at 20 ℃; for 3h;