Methanediol, (2,6-dichlorophenyl)-, diacetate

Base Information

• Chemical Name: Methanediol, (2,6-dichlorophenyl)-, diacetate
• CAS No.: 24653-82-5
• Molecular Formula: C11H10Cl2O4
• Molecular Weight: 277.104
• DSSTox Substance ID: DTXSID701224662
• Nikkaji Number: J1.743.879D
• Mol file: 24653-82-5.mol

Synonyms:24653-82-5;DTXSID701224662;Methanediol, 1-(2,6-dichlorophenyl)-, 1,1-diacetate

Chemical Property of Methanediol, (2,6-dichlorophenyl)-, diacetate

Chemical Property:

• XLogP3: 2.9
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 5
• Exact Mass: 275.9956142
• Heavy Atom Count: 17
• Complexity: 269

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(=O)OC(C1=C(C=CC=C1Cl)Cl)OC(=O)C

Technology Process of Methanediol, (2,6-dichlorophenyl)-, diacetate

There total 4 articles about Methanediol, (2,6-dichlorophenyl)-, diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

acetic anhydride (108-24-7) + 2,6-dichlorobenzaldehyde (83-38-5) → 1,1-diacetoxy-1-(2,6-dichlorophenyl)methane (24653-82-5)

Guidance literature:

With p-toluenesulfonic acid-paraformaldehyde copolymer; at 25 ℃; for 0.25h; Neat (no solvent);

DOI:10.3390/molecules15096493

Reference yield:

acetic anhydride (108-24-7) + 2,6-dichlorobenzaldehyde (83-38-5) → (2E)-3-(2,6-dichlorophenyl)prop-2-enoic acid (20595-49-7) + 1,1-diacetoxy-1-(2,6-dichlorophenyl)methane (24653-82-5)

Guidance literature:

With sodium acetate; at 180 ℃;

Reference yield:

sodium acetate (127-09-3) + acetic anhydride (108-24-7) + 2,6-dichlorobenzaldehyde (83-38-5) → (2E)-3-(2,6-dichlorophenyl)prop-2-enoic acid (20595-49-7) + 1,1-diacetoxy-1-(2,6-dichlorophenyl)methane (24653-82-5)

Guidance literature:

at 180 ℃;

upstream raw materials:

sodium acetate

acetic anhydride

2,6-dichlorobenzaldehyde

Downstream raw materials:

(2E)-3-(2,6-dichlorophenyl)prop-2-enoic acid

2,6-dichlorobenzaldehyde

(2,6-dichloro-phenyl)-propiolic acid

2,3-dibromo-3-(2,6-dichloro-phenyl)-propionic acid