Cyclohexane, 1,1-dimethoxy-3,3-dimethyl-

Base Information

• Chemical Name: Cyclohexane, 1,1-dimethoxy-3,3-dimethyl-
• CAS No.: 24770-65-8
• Molecular Formula: C10H20O2
• Molecular Weight: 172.268
• Mol file: 24770-65-8.mol

Synonyms:

Chemical Property of Cyclohexane, 1,1-dimethoxy-3,3-dimethyl-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Cyclohexane, 1,1-dimethoxy-3,3-dimethyl-

There total 1 articles about Cyclohexane, 1,1-dimethoxy-3,3-dimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methanol (67-56-1) + 3,3-dimethylcyclohexanone (2979-19-3) + trimethyl orthoformate (149-73-5) → 1,1-dimethoxy-3,3-dimethyl-cyclohexane (24770-65-8)

Guidance literature:

With toluene-4-sulfonic acid; at 20 ℃; for 12h; Inert atmosphere; Sealed tube;

DOI:10.1002/anie.202107331

Reference yield:

oxisoindole (480-91-1) + vinyl acetate (108-05-4,9003-20-7) + 1,1-dimethoxy-3,3-dimethyl-cyclohexane (24770-65-8) → 2-(5,5-dimethyl-2-vinylcyclohex-1-en-1-yl)isoindolin-1-one

Guidance literature:

oxisoindole; 1,1-dimethoxy-3,3-dimethyl-cyclohexane; With toluene-4-sulfonic acid; In toluene; at 130 ℃; for 12h; Dean-Stark; Sealed tube;

vinyl acetate; With bis(1,5-cyclooctadiene)iridium(I) tetrakis[3,5-bis(trifluoromethyl)phenyl]borate; o-phenylenebis(diphenylphosphine); In 1,4-dioxane; at 150 ℃; for 24h; Inert atmosphere; Sealed tube;

DOI:10.1002/anie.202107331

Reference yield:

oxisoindole (480-91-1) + 1,1-dimethoxy-3,3-dimethyl-cyclohexane (24770-65-8) → 2-(5,5-dimethylcyclohex-1-en-1-yl)isoindolin-1-one + C16H19NO

Guidance literature:

With toluene-4-sulfonic acid; In toluene; at 130 ℃; for 12h; Overall yield = 150 mg; Dean-Stark; Inert atmosphere; Sealed tube;

DOI:10.1002/anie.202107331

upstream raw materials:

methanol

3,3-dimethylcyclohexanone

trimethyl orthoformate