Ethyl 2,3-dicyano-3-phenylpropanoate

Base Information

Chemical Name:Ethyl 2,3-dicyano-3-phenylpropanoate
CAS No.:5473-13-2
Molecular Formula:C13H12 N2 O2
Molecular Weight:228.25
Hs Code.:
NSC Number:29656
DSSTox Substance ID:DTXSID40283097

Synonyms:ethyl 2,3-dicyano-3-phenylpropanoate;5473-13-2;NSC29656;DTXSID40283097;ethyl2,3-dicyano-3-phenylpropanoate;NSC 29656;NSC-29656;AKOS015917617;NCGC00338994-01;CS-0245548;FT-0654933;EN300-30646;2,3-dicyano-3-phenyl-propionic acid ethyl ester;AB01330713-02;A830349;Z315899006

Suppliers and Price of Ethyl 2,3-dicyano-3-phenylpropanoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of Ethyl 2,3-dicyano-3-phenylpropanoate

Chemical Property:

Vapor Pressure:2.36E-07mmHg at 25°C
Boiling Point:422.7°Cat760mmHg
Flash Point:184.8°C
Density:1.163g/cm³
XLogP3:1.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:5
Exact Mass:228.089877630
Heavy Atom Count:17
Complexity:354

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)C(C#N)C(C#N)C1=CC=CC=C1

Technology Process of Ethyl 2,3-dicyano-3-phenylpropanoate

There total 11 articles about Ethyl 2,3-dicyano-3-phenylpropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 2025-40-3
ethyl benzylidenecyanoacetate

: potassium ferrocyanide

: 5473-13-2
ethyl 2,3-dicyano-3-phenylpropanoate

Guidance literature:: potassium ferrocyanide; With benzoyl chloride; at 160 ℃; for 3h; Green chemistry;

ethyl benzylidenecyanoacetate; With potassium carbonate; In ethanol; at 20 ℃; for 4h; Reagent/catalyst; Solvent; chemoselective reaction; Green chemistry;
DOI:10.1515/chempap-2015-0055

Reference yield:

: 100-52-7
benzaldehyde

: 5473-13-2
ethyl 2,3-dicyano-3-phenylpropanoate

Guidance literature:: Multi-step reaction with 2 steps

1: piperidine / ethanol / 35 - 65 °C

2: 1 h / 35 - 80 °C

With piperidine; In ethanol;
DOI:10.1016/j.bmcl.2006.06.035

Reference yield:

: 105-56-6
ethyl 2-cyanoacetate

: 5473-13-2
ethyl 2,3-dicyano-3-phenylpropanoate

Guidance literature:: Multi-step reaction with 2 steps

1: piperidine / ethanol / 35 - 65 °C

2: 1 h / 35 - 80 °C

With piperidine; In ethanol;
DOI:10.1016/j.bmcl.2006.06.035