2-[4-(2,4-DINITROPHENYL)PIPERAZIN-1-YL]ETHANOL

Base Information

Chemical Name:2-[4-(2,4-DINITROPHENYL)PIPERAZIN-1-YL]ETHANOL
CAS No.:331652-62-1
Molecular Formula:C12H16N4O5
Molecular Weight:296.27900
Hs Code.:
Mol file:331652-62-1.mol

Synonyms:2-[4-(2,4-Dinitro-phenyl)-piperazin-1-yl]-ethanol;N-<2,4-Dinitro-phenyl>-N'-<2-hydroxyaethyl>-piperazin;

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-[4-(2,4-DINITROPHENYL)PIPERAZIN-1-YL]ETHANOL

Chemical Property:

Melting Point:92 °C
Boiling Point:503.9±50.0 °C(Predicted)
PKA:14.96±0.10(Predicted)
PSA：118.35000
Density:1.400±0.06 g/cm3(Predicted)
LogP:1.66660

Purity/Quality:

Safty Information:

Pictogram(s):
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Technology Process of 2-[4-(2,4-DINITROPHENYL)PIPERAZIN-1-YL]ETHANOL

There total 11 articles about 2-[4-(2,4-DINITROPHENYL)PIPERAZIN-1-YL]ETHANOL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 103-76-4
1-(2-hydroxyethyl)piperazine

: 70-34-8,65727-75-5
2,4-Dinitrofluorobenzene

: 331652-62-1
2-[4-(2,4-dinitrophenyl)piperazin-1-yl]ethanol

Guidance literature:: In dichloromethane; for 0.25h;
DOI:10.1021/jo061900m

Reference yield:

: 51-28-5
2,4-Dinitrophenol

: 331652-62-1
2-[4-(2,4-dinitrophenyl)piperazin-1-yl]ethanol

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / N,N-dimethyl-formamide / 80 °C / Inert atmosphere

2: ethanol; water / 25 °C / pH 9.39

With triethylamine; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1002/kin.20756

Reference yield:

: 54436-53-2
O,O-diethyl (2,4-dinitrophenyl) phosphate triester

: 331652-62-1
2-[4-(2,4-dinitrophenyl)piperazin-1-yl]ethanol

Guidance literature:: Multi-step reaction with 3 steps

1: ethanol; water / 25 °C / pH 8.48

2: triethylamine / N,N-dimethyl-formamide / 80 °C / Inert atmosphere

3: ethanol; water / 25 °C / pH 9.39

With triethylamine; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1002/kin.20756