Benzoic acid, 2,2-diethylhydrazide

Base Information

Chemical Name:Benzoic acid, 2,2-diethylhydrazide
CAS No.:33233-39-5
Molecular Formula:C11H16N2O
Molecular Weight:192.261
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzoic acid, 2,2-diethylhydrazide

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Technology Process of Benzoic acid, 2,2-diethylhydrazide

There total 6 articles about Benzoic acid, 2,2-diethylhydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 64-17-5
ethanol

: 613-94-5
benzoic acid hydrazide

: 33233-39-5
N′,N′-diethylbenzohydrazide

Guidance literature:: With [carbonylchlorohydrido{bis[2-(diphenylphosphinomethyl)ethyl]amino}ethylamino] ruthenium(II); potassium tert-butylate; In toluene; at 135 ℃; for 24h; chemoselective reaction; Schlenk technique; Inert atmosphere; Green chemistry;
DOI:10.1021/acs.orglett.0c02369

Reference yield: 58.0%

: 74-96-4
ethyl bromide

: 613-94-5
benzoic acid hydrazide

: 33233-39-5
N′,N′-diethylbenzohydrazide

Guidance literature:: With potassium hydroxide; In isopropyl alcohol; Heating;
DOI:10.1134/S1070427207100370

Reference yield:

: 64-67-5
diethyl sulfate

: 613-94-5
benzoic acid hydrazide

: 14674-46-5
N-benzoyl-N'-ethylhydrazine

: 33233-39-5
N′,N′-diethylbenzohydrazide

Guidance literature:: diethyl sulfate; benzoic acid hydrazide; at 20 ℃; for 18h; Cooling;

With 4-methoxy-benzaldehyde; acetic acid; In ethanol; water; for 1h;
DOI:10.1016/j.bmcl.2019.06.006