potassiumato (E)-methyldiazenolatato

Base Information

• Chemical Name: potassiumato (E)-methyldiazenolatato
• CAS No.: 87039-32-5
• Molecular Formula: CH₃N₂O*K
• Molecular Weight: 98.1459

Synonyms:

Chemical Property of potassiumato (E)-methyldiazenolatato

Chemical Property:

• Vapor Pressure: 40.2mmHg at 25°C
• Boiling Point: 87.3°Cat760mmHg
• Flash Point: 17.3°C
• Density: g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of potassiumato (E)-methyldiazenolatato

There total 5 articles about potassiumato (E)-methyldiazenolatato which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

methylhydrazine (60-34-4) → potassium methyl(nitroso)amide (87039-32-5)

Guidance literature:

With potassium ethoxide; isopentyl nitrite; In diethyl ether; ethanol; at 20 ℃; for 3h;

DOI:10.1002/zaac.201100446

Reference yield:

methylhydrazine (60-34-4) → (E)-potassium methanediazotate (87039-32-5,98114-62-6,3058-37-5)

Guidance literature:

With ethyl nitrite; potassium ethoxide; In diethyl ether; ethanol; at 0 ℃; for 2h;

DOI:10.1016/S1383-5718(97)00180-0

Reference yield:

methanol (67-56-1) → (E)-potassium methanediazotate (87039-32-5,98114-62-6,3058-37-5)

Guidance literature:

With sodium hydroxide; sodium perchlorate; at 25 ℃; Equilibrium constant; var. buffers;

DOI:10.1021/ja00027a060

upstream raw materials:

methylamine

methylhydrazine

methanol

Downstream raw materials:

methanol

Benzylmethylnitrosamin

benzyl-ONN-azoxymethane

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