Benzenesulfonamide, N-3-butenyl-4-methyl-N-2-propenyl-

Base Information

Chemical Name:Benzenesulfonamide, N-3-butenyl-4-methyl-N-2-propenyl-
CAS No.:483370-09-8
Molecular Formula:C14H19NO2S
Molecular Weight:265.376
Hs Code.:
DSSTox Substance ID:DTXSID50465882
Nikkaji Number:J1.894.240B
Wikidata:Q82292169

Synonyms:483370-09-8;Benzenesulfonamide, N-3-butenyl-4-methyl-N-2-propenyl-;N-but-3-enyl-4-methyl-N-prop-2-enylbenzenesulfonamide;SCHEMBL1931740;DTXSID50465882;AKOS028114159;FT-0738954

Suppliers and Price of Benzenesulfonamide, N-3-butenyl-4-methyl-N-2-propenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of Benzenesulfonamide, N-3-butenyl-4-methyl-N-2-propenyl-

Chemical Property:

XLogP3:3.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:7
Exact Mass:265.11365002
Heavy Atom Count:18
Complexity:362

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)S(=O)(=O)N(CCC=C)CC=C

Technology Process of Benzenesulfonamide, N-3-butenyl-4-methyl-N-2-propenyl-

There total 6 articles about Benzenesulfonamide, N-3-butenyl-4-methyl-N-2-propenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 5162-44-7
1-bromo-4-butene

: 50487-71-3
4-methyl-N-(2-propenyl)benzenesulfonamide

: 483370-09-8
N-allyl-N-but-3-enyl-4-methyl-benzenesulfonamide

Guidance literature:: With potassium carbonate; In acetonitrile; for 6h; Heating;
DOI:10.1002/anie.200454157

Reference yield: 83.0%

: C₁₃H₁₆N₄O₂S

: 762-72-1
allyl-trimethyl-silane

: 483370-09-8
N-allyl-N-but-3-enyl-4-methyl-benzenesulfonamide

Guidance literature:: With boron trifluoride diethyl etherate; In toluene; at 30 ℃;
DOI:10.1021/acs.orglett.8b03062

Reference yield:

: 18303-04-3
N-[(tert-butoxy)carbonyl]-4-methylbenzenesulfonamide

: 483370-09-8
N-allyl-N-but-3-enyl-4-methyl-benzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / K₂CO₃ / acetonitrile / 1.5 h / Heating

2: 306.2 mg / TFA / CH₂Cl₂ / 40 h / 20 °C

3: 89 percent / K₂CO₃ / acetonitrile / 6 h / Heating

With potassium carbonate; trifluoroacetic acid; In dichloromethane; acetonitrile;
DOI:10.1002/anie.200454157