9H-Carbazole, 9-(1-ethoxyethyl)-

Base Information

• Chemical Name: 9H-Carbazole, 9-(1-ethoxyethyl)-
• CAS No.: 5509-27-3
• Molecular Formula: C16H17NO
• Molecular Weight: 239.317
• DSSTox Substance ID: DTXSID00396995
• Mol file: 5509-27-3.mol

Synonyms:9H-Carbazole, 9-(1-ethoxyethyl)-;5509-27-3;9-(a-ethoxyethyl) carbazole;DTXSID00396995;9-(1-ethoxyethyl)-9H-carbazole;STL328001;AKOS022108407

Chemical Property of 9H-Carbazole, 9-(1-ethoxyethyl)-

Chemical Property:

• XLogP3: 4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 3
• Exact Mass: 239.131014166
• Heavy Atom Count: 18
• Complexity: 258

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCOC(C)N1C2=CC=CC=C2C3=CC=CC=C31

Technology Process of 9H-Carbazole, 9-(1-ethoxyethyl)-

There total 2 articles about 9H-Carbazole, 9-(1-ethoxyethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 5.0%

9-vinyl-9H-carbazole (1484-13-5,25067-59-8) + ethanol (64-17-5) + benzaldehyde (100-52-7) + 4-methoxy-aniline (104-94-9) → cis-4-(carbazol-9-yl)-6-methoxy-2-phenyl-1,2,3,4-tetrahydroquinoline + trans-4-(carbazol-9-yl)-6-methoxy-2-phenyl-1,2,3,4-tetrahydroquinoline + 9-(1-ethoxyethyl)-9H-carbazole (5509-27-3) + C30H30N2O2

Guidance literature:

With 10,11-dimethyl-8,9,12,13-tetrahydrodiisoquinolino[1,2-a:2′,1′-k][2,9]phenanthroline-7,14-diium trifluoromethanesulfonate; In acetonitrile; at 50 ℃; for 48h;

DOI:10.1002/cplu.202000151

Reference yield:

diethyl acetal (105-57-7,30846-29-8) + 9H-carbazole (86-74-8,105184-46-1,97960-57-1) → ethanol (64-17-5) + 9-(1-ethoxyethyl)-9H-carbazole (5509-27-3)

Guidance literature:

With sulfuric acid; In 1,4-dioxane; at 15 ℃; Product distribution; Mechanism; Rate constant;

upstream raw materials:

diethyl acetal

9H-carbazole

9-vinyl-9H-carbazole

ethanol