4-Hepten-3-ol, 2-methyl-6-(phenylmethoxy)-, (3R,4Z,6R)-

Base Information

Chemical Name:4-Hepten-3-ol, 2-methyl-6-(phenylmethoxy)-, (3R,4Z,6R)-
CAS No.:562071-90-3
Molecular Formula:C15H22O2
Molecular Weight:234.338
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-Hepten-3-ol, 2-methyl-6-(phenylmethoxy)-, (3R,4Z,6R)-

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Technology Process of 4-Hepten-3-ol, 2-methyl-6-(phenylmethoxy)-, (3R,4Z,6R)-

There total 2 articles about 4-Hepten-3-ol, 2-methyl-6-(phenylmethoxy)-, (3R,4Z,6R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 78-84-2
isobutyraldehyde

: 477288-58-7
(R)-((but-3-yn-2-yloxy)methyl)benzene

: 562071-90-3
(3R,4Z,6R)-6-benzyloxy-2-methylhept-4-en-3-ol

: 562071-95-8
(3S,4Z,6R)-6-benzyloxy-2-methylhept-4-en-3-ol

Guidance literature:: (R)-((but-3-yn-2-yloxy)methyl)benzene; With (-)-N-methylephedrine; zinc trifluoromethanesulfonate; triethylamine; In toluene; at 20 ℃; for 0.5h;

isobutyraldehyde; In toluene; at 65 ℃; for 1h;

With quinoline; hydrogen; Lindlar's catalyst; In ethyl acetate; at 20 ℃; for 1h; under 760 Torr;
DOI:10.1016/S0957-4166(03)00120-4

Reference yield:

: 100-39-0
benzyl bromide

: 562071-90-3
(3R,4Z,6R)-6-benzyloxy-2-methylhept-4-en-3-ol

Guidance literature:: Multi-step reaction with 2 steps

1.1: NaH; tetrabutylammonium iodide / tetrahydrofuran / 0.75 h

1.2: 83 percent / tetrahydrofuran / 20 °C

2.1: Zn(OTf)2; (-)-N-methylephedrine; Et₃N / toluene / 0.5 h / 20 °C

2.2: toluene / 1 h / 65 °C

2.3: H₂; quinoline / Lindlar catalyst / ethyl acetate / 1 h / 20 °C / 760 Torr

With (-)-N-methylephedrine; tetra-(n-butyl)ammonium iodide; zinc trifluoromethanesulfonate; sodium hydride; triethylamine; In tetrahydrofuran; toluene;
DOI:10.1016/S0957-4166(03)00120-4

Reference yield: 66.0%

: 562071-90-3
(3R,4Z,6R)-6-benzyloxy-2-methylhept-4-en-3-ol

: (3S,6R)-2-benzyloxy-6-methylheptan-5-ol

Guidance literature:: With hydrogen; platinum on activated charcoal; In ethyl acetate; at 20 ℃; for 1h; under 760 Torr;
DOI:10.1016/S0957-4166(03)00120-4