Holmium antimonide

Base Information

• Chemical Name: Holmium antimonide
• CAS No.: 12029-86-6
• Molecular Formula: HoSb+3
• Molecular Weight: 286.6887
• European Community (EC) Number: 234-738-1
• Mol file: 12029-86-6.mol

Synonyms:Holmium antimonide;antimony;holmium(3+);EINECS 234-738-1;12029-86-6;Antimony, compound with holmium (1:1);Ho.Sb;Holmium antimonide (HoSb)

Chemical Property of Holmium antimonide

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• Density: g/cm³
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 0
• Exact Mass: 285.83414
• Heavy Atom Count: 2
• Complexity: 0

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: [Sb].[Ho+3]

Technology Process of Holmium antimonide

There total 4 articles about Holmium antimonide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

holmium (13598-41-9,13967-65-2,14391-20-9,15125-75-4,15700-49-9,15749-97-0,15750-02-4,15832-34-5,7440-60-0) + antimony (7440-36-0) → holmium monoantimonide (12029-86-6)

Guidance literature:

In neat (no solvent); Ho metal filings and elemental Sb in 1:1 molar ratio pressed, sealed (vac.), heated to 600°C (50°C/h), kept for 12 h, heated to 850°C (50°C/h), kept for 48 h; cooled (air);

DOI:10.1002/ejic.201100313

Reference yield:

holmium (13598-41-9,13967-65-2,14391-20-9,15125-75-4,15700-49-9,15749-97-0,15750-02-4,15832-34-5,7440-60-0) + antimony (7440-36-0) + calcium (7440-70-2) → Ca11Sb10 + holmium monoantimonide (12029-86-6) + Ca3.07Ho0.93Sb3

Guidance literature:

With lead; at 999.84 ℃; for 72h; Inert atmosphere; Glovebox; Sealed tube;

DOI:10.1021/acs.chemmater.1c03300

Reference yield:

holmium (13598-41-9,13967-65-2,14391-20-9,15125-75-4,15700-49-9,15749-97-0,15750-02-4,15832-34-5,7440-60-0) + antimony (7440-36-0) → HoSb, low pressure (12029-86-6)

Guidance literature:

In neat (no solvent); reaction of metal and antimony in sealed tube at 800°C;

upstream raw materials:

holmium

antimony

iron

calcium