Technology Process of hydroxypentanone,3-hydroxy-2-pentanone
There total 46 articles about hydroxypentanone,3-hydroxy-2-pentanone which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
calcium carbonate; methyl iodide;
In
acetone;
for 24h;
Heating;
- Guidance literature:
-
pentan-3-one;
With
potassium hydroxide;
In
methanol;
for 0.25h;
Inert atmosphere;
Cooling with ice;
With
[bis(acetoxy)iodo]benzene;
In
methanol;
at 0 - 20 ℃;
for 12.5h;
Inert atmosphere;
With
sulfuric acid;
In
methanol; water;
at 20 ℃;
for 0.25h;
Inert atmosphere;
DOI:10.1016/j.tetlet.2017.03.053
- Guidance literature:
-
methanol; 2-Pentanone;
With
potassium hydroxide;
for 0.25h;
Inert atmosphere;
Cooling with ice;
With
[bis(acetoxy)iodo]benzene;
at 0 - 20 ℃;
for 12.5h;
Inert atmosphere;
With
sulfuric acid;
In
water;
at 20 ℃;
for 0.25h;
Inert atmosphere;
DOI:10.1016/j.tetlet.2017.03.053
