Bicyclo[2.2.1]heptane-2,3,5-tricarboxylic acid, 7-(phenylmethoxy)-6-[[[2-(trimethylsilyl)ethoxy]carbonyl]amino]-, 2,3-dimethyl 5-[(1R,2S,5R)-5-methyl-2-(1-methylethyl)cyclohexyl] ester, (1S,2R,3S,4R,5S,6S,7S)-

Base Information

Chemical Name:Bicyclo[2.2.1]heptane-2,3,5-tricarboxylic acid, 7-(phenylmethoxy)-6-[[[2-(trimethylsilyl)ethoxy]carbonyl]amino]-, 2,3-dimethyl 5-[(1R,2S,5R)-5-methyl-2-(1-methylethyl)cyclohexyl] ester, (1S,2R,3S,4R,5S,6S,7S)-
CAS No.:581100-23-4
Molecular Formula:C35H53NO9Si
Molecular Weight:659.893
Hs Code.:

Bicyclo[2.2.1]heptane-2,3,5-tricarboxylic acid,
7-(phenylmethoxy)-6-[[[2-(trimethylsilyl)ethoxy]carbonyl]amino]-,
2,3-dimethyl 5-[(1R,2S,5R)-5-methyl-2-(1-methylethyl)cyclohexyl] ester,
(1S,2R,3S,4R,5S,6S,7S)-

Synonyms:

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Chemical Property of Bicyclo[2.2.1]heptane-2,3,5-tricarboxylic acid, 7-(phenylmethoxy)-6-[[[2-(trimethylsilyl)ethoxy]carbonyl]amino]-, 2,3-dimethyl 5-[(1R,2S,5R)-5-methyl-2-(1-methylethyl)cyclohexyl] ester, (1S,2R,3S,4R,5S,6S,7S)-

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Technology Process of Bicyclo[2.2.1]heptane-2,3,5-tricarboxylic acid, 7-(phenylmethoxy)-6-[[[2-(trimethylsilyl)ethoxy]carbonyl]amino]-, 2,3-dimethyl 5-[(1R,2S,5R)-5-methyl-2-(1-methylethyl)cyclohexyl] ester, (1S,2R,3S,4R,5S,6S,7S)-

There total 1 articles about Bicyclo[2.2.1]heptane-2,3,5-tricarboxylic acid, 7-(phenylmethoxy)-6-[[[2-(trimethylsilyl)ethoxy]carbonyl]amino]-, 2,3-dimethyl 5-[(1R,2S,5R)-5-methyl-2-(1-methylethyl)cyclohexyl] ester, (1S,2R,3S,4R,5S,6S,7S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67-56-1
methanol

: 581100-22-3
bicyclo[2.2.1]hept-5-ene-7-syn-(benzyloxy)-2-exo-(trimethylsilylethoxycarbonyl)-amino-3-endo-(L)-menthyl carboxylate

: 201230-82-2
carbon monoxide

: 581100-23-4
bicyclo[2.2.1]heptane-7-syn-(benzyloxy)-2-exo-(trimethylsilylethoxycarbonyl)-amino-3-endo-(L)-menthyl-5-exo-methyl-6-exo-methyl tricarboxylate

Guidance literature:: With copper dichloride; palladium 10% on activated carbon; for 72h; under 760.051 Torr;

Reference yield:

: 581100-23-4
bicyclo[2.2.1]heptane-7-syn-(benzyloxy)-2-exo-(trimethylsilylethoxycarbonyl)-amino-3-endo-(L)-menthyl-5-exo-methyl-6-exo-methyl tricarboxylate

: 581100-24-5
bicyclo[2.2.1]heptane-7-syn-(benzyloxy)-2-exo-(trimethylsilylethoxycarbonyl)-amino-3-endo-(L)-menthylcarbox-5-exo-6-exo-dicarboxylic anhydride

Guidance literature:: bicyclo[2.2.1]heptane-7-syn-(benzyloxy)-2-exo-(trimethylsilylethoxycarbonyl)-amino-3-endo-(L)-menthyl-5-exo-methyl-6-exo-methyl tricarboxylate; With formic acid; toluene-4-sulfonic acid; at 90 ℃;

With acetic anhydride; In formic acid; for 6h; Heating / reflux;