methyl 2-(acetylamino)-2-deoxy-3,4,6-tri-O-methylhexopyranoside

Base Information

• Chemical Name: methyl 2-(acetylamino)-2-deoxy-3,4,6-tri-O-methylhexopyranoside
• CAS No.: 6195-86-4
• Molecular Formula: C₁₂H₂₃NO₆
• Molecular Weight: 277.318

Synonyms:Glucopyranoside,methyl 2-acetamido-2-deoxy-3,4,6-tri-O-methyl- (6CI); Glucopyranoside, methyl2-acetamido-2-deoxy-3,4,6-tri-O-methyl-, b-D- (8CI); NSC 248993

Chemical Property of methyl 2-(acetylamino)-2-deoxy-3,4,6-tri-O-methylhexopyranoside

Chemical Property:

• Vapor Pressure: 2.05E-07mmHg at 25°C
• Boiling Point: 424.5°Cat760mmHg
• Flash Point: 210.6°C
• Density: 1.12g/cm³

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
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MSDS Files:

SDS file from LookChem

Useful:

Technology Process of methyl 2-(acetylamino)-2-deoxy-3,4,6-tri-O-methylhexopyranoside

There total 6 articles about methyl 2-(acetylamino)-2-deoxy-3,4,6-tri-O-methylhexopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl-[O3,O4,O6-trimethyl-O2-(toluene-4-sulfonyl)-β-D-galactopyranoside] (36480-32-7) → methyl-(2-acetylamino-O3,O4,O6-trimethyl-2-deoxy-β-D-talopyranoside) (6195-86-4,7323-01-5,7380-60-1,7384-32-9,7437-12-9,7437-13-0,10049-88-4,42756-56-9,96744-17-1,110715-58-7)

Guidance literature:

With methanol; ammonia; Behandeln des Reaktionsprodukts in Methanol mit Acetanhydrid;

DOI:10.1039/jr9440000522

Reference yield:

methanol (67-56-1) + ammonia (7664-41-7) + methyl-[O3,O4,O6-trimethyl-O2-(toluene-4-sulfonyl)-β-D-galactopyranoside] (36480-32-7) → methyl-(2-acetylamino-O3,O4,O6-trimethyl-2-deoxy-β-D-talopyranoside) (6195-86-4,7323-01-5,7380-60-1,7384-32-9,7437-12-9,7437-13-0,10049-88-4,42756-56-9,96744-17-1,110715-58-7)

Guidance literature:

at 200 ℃; Behandeln des Reaktionsprodukts in Methanol mit Acetanhydrid;

DOI:10.1039/jr9440000522

Reference yield:

2-acetamido-3,4,6-tri-O-acetyl-D-glucopyranosyl acetate (3006-60-8,4539-83-7,6730-10-5,7772-79-4,7784-54-5,10385-50-9,26151-16-6,76375-60-5,76375-61-6,95341-98-3,95341-99-4,134451-91-5,134451-96-0,136982-81-5,145375-11-7,148347-15-3,14086-90-9) + dimethyl sulfate (77-78-1) → methyl 2-acetamido-2-deoxy-3,4,6-tri-O-methyl-β-D-glucopyranoside (6195-86-4)

Guidance literature:

With methanol; tetrachloromethane; sodium hydroxide;

upstream raw materials:

methyl-[O³,O⁴,O⁶-trimethyl-O²-(toluene-4-sulfonyl)-β-D-galactopyranoside]

methanol

ammonia

2-acetamido-3,4,6-tri-O-acetyl-D-glucopyranosyl acetate

Downstream raw materials:

methyl 2-acetamido-3,4,6-tri-O-methyl-2-deoxy-α-D-glucopyranoside

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