Methyl 2-(acetylamino)-3-O,4-O,6-O-trimethyl-2-deoxy-α-D-glucopyranoside

Base Information

• Chemical Name: Methyl 2-(acetylamino)-3-O,4-O,6-O-trimethyl-2-deoxy-α-D-glucopyranoside
• CAS No.: 7380-60-1
• Molecular Formula: C12H23NO6
• Molecular Weight: 277.31
• Mol file: 7380-60-1.mol

Synonyms:Methyl 2-(acetylamino)-3-O,4-O,6-O-trimethyl-2-deoxy-α-D-glucopyranoside

Chemical Property of Methyl 2-(acetylamino)-3-O,4-O,6-O-trimethyl-2-deoxy-α-D-glucopyranoside

Chemical Property:

• PSA: 75.25000
• LogP: -0.07030

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of Methyl 2-(acetylamino)-3-O,4-O,6-O-trimethyl-2-deoxy-α-D-glucopyranoside

There total 14 articles about Methyl 2-(acetylamino)-3-O,4-O,6-O-trimethyl-2-deoxy-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl-[O3,O4,O6-trimethyl-O2-(toluene-4-sulfonyl)-β-D-galactopyranoside] (36480-32-7) → methyl-(2-acetylamino-O3,O4,O6-trimethyl-2-deoxy-β-D-talopyranoside) (6195-86-4,7323-01-5,7380-60-1,7384-32-9,7437-12-9,7437-13-0,10049-88-4,42756-56-9,96744-17-1,110715-58-7)

Guidance literature:

With methanol; ammonia; Behandeln des Reaktionsprodukts in Methanol mit Acetanhydrid;

DOI:10.1039/jr9440000522

Reference yield:

methanol (67-56-1) + ammonia (7664-41-7) + methyl-[O3,O4,O6-trimethyl-O2-(toluene-4-sulfonyl)-β-D-galactopyranoside] (36480-32-7) → methyl-(2-acetylamino-O3,O4,O6-trimethyl-2-deoxy-β-D-talopyranoside) (6195-86-4,7323-01-5,7380-60-1,7384-32-9,7437-12-9,7437-13-0,10049-88-4,42756-56-9,96744-17-1,110715-58-7)

Guidance literature:

at 200 ℃; Behandeln des Reaktionsprodukts in Methanol mit Acetanhydrid;

DOI:10.1039/jr9440000522

Reference yield:

Methyl 2-acetamido-2-deoxy-3,4-di-O-methyl-α-D-glucopyranoside (63573-30-8) + methyl iodide (74-88-4) → methyl 2-acetamido-3,4,6-tri-O-methyl-2-deoxy-α-D-glucopyranoside (7380-60-1)

Guidance literature:

With silver(l) oxide;

DOI:10.1021/ja01138a045

upstream raw materials:

methyl-[O³,O⁴,O⁶-trimethyl-O²-(toluene-4-sulfonyl)-β-D-galactopyranoside]

methanol

ammonia

dimethyl sulfate

Downstream raw materials:

methyl 2-(acetylmethylamino)-2-deoxy-3,4,6-tri-O-methyl-α-D-glucopyranoside

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