1-Methyl-4-[(E)-styryl]-1,2,3,6-tetrahydropyridine

Base Information

Chemical Name:1-Methyl-4-[(E)-styryl]-1,2,3,6-tetrahydropyridine
CAS No.:130407-16-8
Molecular Formula:C₁₄H₁₇N
Molecular Weight:199.296
Hs Code.:
Nikkaji Number:J358.512C,J515.460J
Mol file:130407-16-8.mol

Synonyms:1-methyl-1,2,3,6-tetrahydrostilbazole;1-MTHS;1-MTHSZ

Suppliers and Price of 1-Methyl-4-[(E)-styryl]-1,2,3,6-tetrahydropyridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 1-Methyl-4-[(E)-styryl]-1,2,3,6-tetrahydropyridine

Chemical Property:

Vapor Pressure:0.000316mmHg at 25°C
Boiling Point:320.5°C at 760 mmHg
Flash Point:134.3°C
PSA：3.24000
Density:1.066g/cm³
LogP:2.89960
XLogP3:3.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:199.136099547
Heavy Atom Count:15
Complexity:246

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN1CCC(=CC1)C=CC2=CC=CC=C2
Isomeric SMILES:CN1CCC(=CC1)/C=C/C2=CC=CC=C2

Technology Process of 1-Methyl-4-[(E)-styryl]-1,2,3,6-tetrahydropyridine

There total 4 articles about 1-Methyl-4-[(E)-styryl]-1,2,3,6-tetrahydropyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 20111-34-6
(E)-1-methyl-4-(2-phenylethenyl)pyridinium iodide

: 130407-16-8
(E)-1-methyl-4-(2-phenylethenyl)-1,2,3,6-tetrahydropyridine

Guidance literature:: With sodium tetrahydroborate; In methanol; for 0.5h; Ambient temperature;
DOI:10.1021/jm00100a023

Reference yield:

: 108-89-4
picoline

: 130407-16-8
(E)-1-methyl-4-(2-phenylethenyl)-1,2,3,6-tetrahydropyridine

Guidance literature:: Multi-step reaction with 2 steps

1: 49 percent / acetic anhydride / 24 h / Heating

2: 2.) NaBH₄ / 1.) acetone, RT, 16 h, 2.) MeOH, RT, 16 h

With sodium tetrahydroborate; acetic anhydride;
DOI:10.1021/jm00174a007

Reference yield:

: 100-52-7
benzaldehyde

: 130407-16-8
(E)-1-methyl-4-(2-phenylethenyl)-1,2,3,6-tetrahydropyridine

Guidance literature:: Multi-step reaction with 2 steps

1: 49 percent / acetic anhydride / 24 h / Heating

2: 2.) NaBH₄ / 1.) acetone, RT, 16 h, 2.) MeOH, RT, 16 h

With sodium tetrahydroborate; acetic anhydride;
DOI:10.1021/jm00174a007