Benzene, 1-[[[(2Z)-3-iodo-2-butenyl]oxy]methyl]-4-methoxy-

Base Information

Chemical Name:Benzene, 1-[[[(2Z)-3-iodo-2-butenyl]oxy]methyl]-4-methoxy-
CAS No.:612090-71-8
Molecular Formula:C12H15IO2
Molecular Weight:318.154
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzene, 1-[[[(2Z)-3-iodo-2-butenyl]oxy]methyl]-4-methoxy-

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Technology Process of Benzene, 1-[[[(2Z)-3-iodo-2-butenyl]oxy]methyl]-4-methoxy-

There total 2 articles about Benzene, 1-[[[(2Z)-3-iodo-2-butenyl]oxy]methyl]-4-methoxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 89238-99-3
O-(4-methoxybenzyl)-trichloroacetimidate

: 35761-83-2
3-iodo-but-2-ene-1-ol

: 612090-71-8
(Z)-1-((3-iodobut-2-enyloxy)methyl)-4-methoxybenzene

Guidance literature:: With pyridinium p-toluenesulfonate; In dichloromethane; cyclohexane; at 0 ℃; Inert atmosphere;
DOI:10.1021/ol100665m

Reference yield:

: 105-13-5
4-Methoxybenzyl alcohol

: 612090-71-8
(Z)-1-((3-iodobut-2-enyloxy)methyl)-4-methoxybenzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / diethyl ether; mineral oil / 0.5 h / 0 °C

1.2: 0.75 h / 0 °C

2.1: pyridinium p-toluenesulfonate / dichloromethane; cyclohexane / 16 h / 0 - 20 °C / Cooling

With pyridinium p-toluenesulfonate; sodium hydride; In diethyl ether; dichloromethane; cyclohexane; mineral oil;
DOI:10.1002/chem.201202553