3,7-bis-(4-trifluoromethylphenyl)-1,5,3,7-dioxadiazocane

Base Information

Chemical Name:3,7-bis-(4-trifluoromethylphenyl)-1,5,3,7-dioxadiazocane
CAS No.:77767-16-9
Molecular Formula:C₁₈H₁₆F₆N₂O₂
Molecular Weight:406.328
Hs Code.:2933990090
Mol file:77767-16-9.mol

Synonyms:3,7-Bis(4-trifluoromethylphenyl)-1,5,3,7-dioxadiazocane

Suppliers and Price of 3,7-bis-(4-trifluoromethylphenyl)-1,5,3,7-dioxadiazocane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 3,7-bis-(4-trifluoromethylphenyl)-1,5,3,7-dioxadiazocane

Chemical Property:

Vapor Pressure:2.42E-09mmHg at 25°C
Boiling Point:479.1°C at 760 mmHg
Flash Point:243.6°C
PSA：24.94000
Density:1.347g/cm³
LogP:5.04400

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3,7-bis-(4-trifluoromethylphenyl)-1,5,3,7-dioxadiazocane

There total 2 articles about 3,7-bis-(4-trifluoromethylphenyl)-1,5,3,7-dioxadiazocane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 455-14-1
4-trifluoromethylphenylamine

: 77767-16-9
1,5-Bis(4-trifluormethylphenyl)-3,7-dioxa-1,5-diazacyclooctan

Guidance literature:: With sulfuric acid; In 1,4-dioxane; water; for 2h; Ambient temperature;
DOI:10.1002/jlac.198119810202

Reference yield:

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 455-14-1
4-trifluoromethylphenylamine

: 74-89-5
methylamine

: 77767-16-9
1,5-Bis(4-trifluormethylphenyl)-3,7-dioxa-1,5-diazacyclooctan

Guidance literature:: With hydrogenchloride; sodium nitrite; Yield given. Multistep reaction; 1.) Water, 2.) -5 - -10 deg C, 20 min; pH 4-5, 30min; pH 1, 15 min;
DOI:10.1016/S0040-4039(00)98507-1