2,4,6-Trimethoxyphenanthrene

Base Information

• Chemical Name: 2,4,6-Trimethoxyphenanthrene
• CAS No.: 63366-84-7
• Molecular Formula: C₁₇H₁₆O₃
• Molecular Weight: 268.312
• DSSTox Substance ID: DTXSID30557815
• Nikkaji Number: J2.070.612K
• Wikidata: Q82439841
• Mol file: 63366-84-7.mol

Synonyms:2,4,6-TRIMETHOXYPHENANTHRENE;63366-84-7;DTXSID30557815

Chemical Property of 2,4,6-Trimethoxyphenanthrene

Chemical Property:

• XLogP3: 4.3
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 3
• Exact Mass: 268.109944368
• Heavy Atom Count: 20
• Complexity: 319

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC1=CC2=C(C=CC3=CC(=CC(=C32)OC)OC)C=C1

Technology Process of 2,4,6-Trimethoxyphenanthrene

There total 2 articles about 2,4,6-Trimethoxyphenanthrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methanol (67-56-1) + 3,5,4'-trimethoxy-trans-stilbene (22255-22-7) → 2,4,6-trimethoxyphenanthrene (63366-84-7) + (Z)-1-(3,5-dimethoxyphenyl)-2-(4-methoxyphenyl)ethene (94608-23-8) + 2-(3,5-dimethoxyphenyl)-1-(4-methoxyphenyl)-1-methoxyethane

Guidance literature:

for 5h; Further Variations:; time dependence; Product distribution; Photolysis;

DOI:10.1139/v03-072

Reference yield:

2,2,2-trifluoroethanol (75-89-8) + 3,5,4'-trimethoxy-trans-stilbene (22255-22-7) → 2,4,6-trimethoxyphenanthrene (63366-84-7) + (Z)-1-(3,5-dimethoxyphenyl)-2-(4-methoxyphenyl)ethene (94608-23-8) + 2-(3,5-dimethoxyphenyl)-1-(4-methoxyphenyl)-1-(trifluoroethoxy)ethane + 1-(3,5-dimethoxyphenyl)-2-(4-methoxyphenyl)-1-(trifluoroethoxy)ethane

Guidance literature:

for 1h; Further Variations:; time dependence; Product distribution; Photolysis;

DOI:10.1139/v03-072

upstream raw materials:

methanol

3,5,4'-trimethoxy-trans-stilbene

2,2,2-trifluoroethanol