N-(Methoxymethyl)-N-methylbenzamide

Base Information

Chemical Name:N-(Methoxymethyl)-N-methylbenzamide
CAS No.:65000-22-8
Molecular Formula:C10H13NO2
Molecular Weight:179.219
Hs Code.:
DSSTox Substance ID:DTXSID20556357
Nikkaji Number:J3.593.781A
Wikidata:Q82437888

Synonyms:N-(Methoxymethyl)-N-methylbenzamide;65000-22-8;DTXSID20556357

Suppliers and Price of N-(Methoxymethyl)-N-methylbenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of N-(Methoxymethyl)-N-methylbenzamide

Chemical Property:

XLogP3:1.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:179.094628657
Heavy Atom Count:13
Complexity:164

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CN(COC)C(=O)C1=CC=CC=C1

Technology Process of N-(Methoxymethyl)-N-methylbenzamide

There total 3 articles about N-(Methoxymethyl)-N-methylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 67-56-1
methanol

: 6526-66-5
2-amino-N,N-dimethylbenzamide

: 65000-22-8
N-(methoxymethyl)-N-methylbenzamide

Guidance literature:: With tert.-butylnitrite; Eosin Y; toluene-4-sulfonic acid; In nitromethane; at 20 ℃; for 24h; Schlenk technique; Inert atmosphere; Irradiation;
DOI:10.1016/j.tetlet.2016.02.108

Reference yield:

: 118-48-9
isatoic anhydride

: 65000-22-8
N-(methoxymethyl)-N-methylbenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: dmap / acetonitrile / 26 h / 0 - 20 °C / Schlenk technique; Inert atmosphere

2: tert.-butylnitrite; Eosin Y; toluene-4-sulfonic acid / nitromethane / 24 h / 20 °C / Schlenk technique; Inert atmosphere; Irradiation

With dmap; tert.-butylnitrite; Eosin Y; toluene-4-sulfonic acid; In nitromethane; acetonitrile;
DOI:10.1016/j.tetlet.2016.02.108