3-Oxazolidinecarboxylic acid, 4-[[[(1Z,3S)-3-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-1-(methoxycarbonyl) -1-butenyl]amino]carbonyl]-2,2,5-trimethyl-, 1,1-dimethylethyl ester, (4S,5R)-

Base Information

Chemical Name:3-Oxazolidinecarboxylic acid, 4-[[[(1Z,3S)-3-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-1-(methoxycarbonyl) -1-butenyl]amino]carbonyl]-2,2,5-trimethyl-, 1,1-dimethylethyl ester, (4S,5R)-
CAS No.:670233-19-9
Molecular Formula:C34H48N2O7Si
Molecular Weight:624.85
Hs Code.:

3-Oxazolidinecarboxylic acid,
4-[[[(1Z,3S)-3-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-1-(methoxycarbonyl)
-1-butenyl]amino]carbonyl]-2,2,5-trimethyl-, 1,1-dimethylethyl ester,
(4S,5R)-

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Chemical Property of 3-Oxazolidinecarboxylic acid, 4-[[[(1Z,3S)-3-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-1-(methoxycarbonyl) -1-butenyl]amino]carbonyl]-2,2,5-trimethyl-, 1,1-dimethylethyl ester, (4S,5R)-

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Technology Process of 3-Oxazolidinecarboxylic acid, 4-[[[(1Z,3S)-3-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-1-(methoxycarbonyl) -1-butenyl]amino]carbonyl]-2,2,5-trimethyl-, 1,1-dimethylethyl ester, (4S,5R)-

There total 2 articles about 3-Oxazolidinecarboxylic acid, 4-[[[(1Z,3S)-3-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-1-(methoxycarbonyl) -1-butenyl]amino]carbonyl]-2,2,5-trimethyl-, 1,1-dimethylethyl ester, (4S,5R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 87696-33-1
(S)-2-(O-tert-butyldiphenylsilyloxy)propanal

: 670233-18-8
(4S,5R)-4-{[(Diethoxy-phosphoryl)-methoxycarbonyl-methyl]-carbamoyl}-2,2,5-trimethyl-oxazolidine-3-carboxylic acid tert-butyl ester

: 670233-19-9
(4S,5R)-4-[(Z)-(S)-3-(tert-Butyl-diphenyl-silanyloxy)-1-methoxycarbonyl-but-1-enylcarbamoyl]-2,2,5-trimethyl-oxazolidine-3-carboxylic acid tert-butyl ester

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran;
DOI:10.1246/cl.2004.72

Reference yield:

: 143364-85-6
(4S,5R)-3-(tert-butoxycarbonyl)-2,2,5-trimethyl-1,3-oxazolidine-4-carboxylic acid

: 670233-19-9
(4S,5R)-4-[(Z)-(S)-3-(tert-Butyl-diphenyl-silanyloxy)-1-methoxycarbonyl-but-1-enylcarbamoyl]-2,2,5-trimethyl-oxazolidine-3-carboxylic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / DCC; HOBt / dimethylformamide

2: 80 percent / DBU / tetrahydrofuran

With benzotriazol-1-ol; 1,8-diazabicyclo[5.4.0]undec-7-ene; dicyclohexyl-carbodiimide; In tetrahydrofuran; N,N-dimethyl-formamide; 2: Hornor-Emmons reaction;
DOI:10.1246/cl.2004.72