3-Oxazolidinecarboxylic acid, 4-[[[(1Z,3S)-1-carboxy-3-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-1-butenyl] amino]carbonyl]-2,2,5-trimethyl-, 3-(1,1-dimethylethyl) ester, (4S,5R)-

Base Information

Chemical Name:3-Oxazolidinecarboxylic acid, 4-[[[(1Z,3S)-1-carboxy-3-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-1-butenyl] amino]carbonyl]-2,2,5-trimethyl-, 3-(1,1-dimethylethyl) ester, (4S,5R)-
CAS No.:670233-20-2
Molecular Formula:C33H46N2O7Si
Molecular Weight:610.823
Hs Code.:

3-Oxazolidinecarboxylic acid,
4-[[[(1Z,3S)-1-carboxy-3-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-1-butenyl]
amino]carbonyl]-2,2,5-trimethyl-, 3-(1,1-dimethylethyl) ester, (4S,5R)-

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Chemical Property of 3-Oxazolidinecarboxylic acid, 4-[[[(1Z,3S)-1-carboxy-3-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-1-butenyl] amino]carbonyl]-2,2,5-trimethyl-, 3-(1,1-dimethylethyl) ester, (4S,5R)-

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Technology Process of 3-Oxazolidinecarboxylic acid, 4-[[[(1Z,3S)-1-carboxy-3-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-1-butenyl] amino]carbonyl]-2,2,5-trimethyl-, 3-(1,1-dimethylethyl) ester, (4S,5R)-

There total 3 articles about 3-Oxazolidinecarboxylic acid, 4-[[[(1Z,3S)-1-carboxy-3-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-1-butenyl] amino]carbonyl]-2,2,5-trimethyl-, 3-(1,1-dimethylethyl) ester, (4S,5R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 670233-19-9
(4S,5R)-4-[(Z)-(S)-3-(tert-Butyl-diphenyl-silanyloxy)-1-methoxycarbonyl-but-1-enylcarbamoyl]-2,2,5-trimethyl-oxazolidine-3-carboxylic acid tert-butyl ester

: 670233-20-2
(4S,5R)-4-[(Z)-(S)-3-(tert-Butyl-diphenyl-silanyloxy)-1-carboxy-but-1-enylcarbamoyl]-2,2,5-trimethyl-oxazolidine-3-carboxylic acid tert-butyl ester

Guidance literature:: With lithium hydroxide; In 1,4-dioxane; water;
DOI:10.1246/cl.2004.72

Reference yield:

: 143364-85-6
(4S,5R)-3-(tert-butoxycarbonyl)-2,2,5-trimethyl-1,3-oxazolidine-4-carboxylic acid

: 670233-20-2
(4S,5R)-4-[(Z)-(S)-3-(tert-Butyl-diphenyl-silanyloxy)-1-carboxy-but-1-enylcarbamoyl]-2,2,5-trimethyl-oxazolidine-3-carboxylic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / DCC; HOBt / dimethylformamide

2: 80 percent / DBU / tetrahydrofuran

3: 100 percent / LiOH / dioxane; H₂O

With lithium hydroxide; benzotriazol-1-ol; 1,8-diazabicyclo[5.4.0]undec-7-ene; dicyclohexyl-carbodiimide; In tetrahydrofuran; 1,4-dioxane; water; N,N-dimethyl-formamide; 2: Hornor-Emmons reaction;
DOI:10.1246/cl.2004.72

Reference yield:

: 670233-18-8
(4S,5R)-4-{[(Diethoxy-phosphoryl)-methoxycarbonyl-methyl]-carbamoyl}-2,2,5-trimethyl-oxazolidine-3-carboxylic acid tert-butyl ester

: 670233-20-2
(4S,5R)-4-[(Z)-(S)-3-(tert-Butyl-diphenyl-silanyloxy)-1-carboxy-but-1-enylcarbamoyl]-2,2,5-trimethyl-oxazolidine-3-carboxylic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / DBU / tetrahydrofuran

2: 100 percent / LiOH / dioxane; H₂O

With lithium hydroxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; 1,4-dioxane; water; 1: Hornor-Emmons reaction;
DOI:10.1246/cl.2004.72