3,3-Bis(1-methylethyl)-1-phenyl-1-triazene

Base Information

Chemical Name:3,3-Bis(1-methylethyl)-1-phenyl-1-triazene
CAS No.:36719-40-1
Molecular Formula:C12H19N3
Molecular Weight:205.303
Hs Code.:
NSC Number:515224
UNII:KE7AXL427A
Nikkaji Number:J3.348.688J

Synonyms:3,3-Bis(1-methylethyl)-1-phenyl-1-triazene;36719-40-1;1-phenyl-3,3-diisopropyltriazene;1-Triazene, 3,3-bis(1-methylethyl)-1-phenyl-;NSC-515224;1-phenyl-3,3-diisopropyltriaz-1-ene;NSC515224;NSC 515224;N-phenyldiazenyl-N-propan-2-ylpropan-2-amine;KE7AXL427A;SCHEMBL17375285;1-Triazene, 3,3-bis(1-methylethyl)-1-phenyl-, (E)-;67961-23-3

Suppliers and Price of 3,3-Bis(1-methylethyl)-1-phenyl-1-triazene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of 3,3-Bis(1-methylethyl)-1-phenyl-1-triazene

Chemical Property:

Vapor Pressure:0.0081mmHg at 25°C
Boiling Point:267.5°Cat760mmHg
Flash Point:115.6°C
Density:0.95g/cm³
XLogP3:4.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:205.157897619
Heavy Atom Count:15
Complexity:185

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)N(C(C)C)N=NC1=CC=CC=C1

Technology Process of 3,3-Bis(1-methylethyl)-1-phenyl-1-triazene

There total 6 articles about 3,3-Bis(1-methylethyl)-1-phenyl-1-triazene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: C₆H₁₄N₃O^(1-)*Li⁽¹⁺⁾

: 100-59-4
phenylmagnesium chloride

: 36719-40-1
1-phenyl-3,3-diisopropyltriaz-1-ene

Guidance literature:: In tetrahydrofuran; at 50 ℃; for 4h;

Reference yield: 48.0%

: 100-34-5
benzene diazonium chloride

: 108-18-9
diisopropylamine

: 36719-40-1
1-phenyl-3,3-diisopropyltriaz-1-ene

Guidance literature:: With sodium carbonate; In water; at 5 - 10 ℃; for 0.5h;
DOI:10.1135/cccc19940401

Reference yield:

: 108-18-9
diisopropylamine

: 36719-40-1
1-phenyl-3,3-diisopropyltriaz-1-ene

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / hexane / 20 °C / Glovebox; Inert atmosphere; Schlenk technique

1.2: 4 h / 20 °C / Glovebox; Schlenk technique

2.1: tetrahydrofuran / 4 h / 50 °C / Inert atmosphere; Glovebox; Schlenk technique

With n-butyllithium; In tetrahydrofuran; hexane;
DOI:10.1002/anie.201408597