1-Chloro-4-[(4-chlorophenyl)-dimethoxymethyl]benzene

Base Information

• Chemical Name: 1-Chloro-4-[(4-chlorophenyl)-dimethoxymethyl]benzene
• CAS No.: 6861-53-6
• Molecular Formula: C15H14Cl2O2
• Molecular Weight: 297.181
• DSSTox Substance ID: DTXSID90470076
• Nikkaji Number: J1.785.608A
• Wikidata: Q82298048
• Mol file: 6861-53-6.mol

Synonyms:1-chloro-4-[(4-chlorophenyl)-dimethoxymethyl]benzene;6861-53-6;Benzene, 1,1'-(dimethoxymethylene)bis[4-chloro-;SCHEMBL1817529;DTXSID90470076;di(4-chlorophenyl)dimethoxymethane;YIHFJRJJGMMPQD-UHFFFAOYSA-N;bis-(4-chlorophenyl)dimethoxymethane;bis-(4-chlorophenyl)-dimethoxymethane;1-chloro-4-[(4-chlorophenyl)(dimethoxy)methyl]benzene

Chemical Property of 1-Chloro-4-[(4-chlorophenyl)-dimethoxymethyl]benzene

Chemical Property:

• XLogP3: 4.3
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 4
• Exact Mass: 296.0370851
• Heavy Atom Count: 19
• Complexity: 241

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC(C1=CC=C(C=C1)Cl)(C2=CC=C(C=C2)Cl)OC

Technology Process of 1-Chloro-4-[(4-chlorophenyl)-dimethoxymethyl]benzene

There total 9 articles about 1-Chloro-4-[(4-chlorophenyl)-dimethoxymethyl]benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

4,4'-Dichlorobenzophenone (90-98-2) + trimethyl orthoformate (149-73-5) → 4,4’-dichlorobenzophenone dimethyl acetal (6861-53-6)

Guidance literature:

With triethylamine; In methanol; at 20 ℃; for 48h;

DOI:10.1246/cl.150166

Reference yield: 97.0%

methanol (67-56-1) + 4,4'-Dichlorobenzophenone (90-98-2) → 4,4’-dichlorobenzophenone dimethyl acetal (6861-53-6)

Guidance literature:

With trimethyl orthoformate; for 24h; Heating;

DOI:10.1080/00397910802219361

Reference yield: 75.0%

methanol (67-56-1) + 4,4'-dichlorobenzophenone hydrazone (5463-11-6) → 4,4'-dichlorodiphenylmethane (101-76-8) + 4,4’-dichlorobenzophenone dimethyl acetal (6861-53-6) + Bis(4-chlorophenyl)methyl methyl ether (55702-41-5)

Guidance literature:

With sodium methylate; at 17 ℃; for 3h; Pt-anode, applied potl. vs. SCE 0.9-1.0 V, 3.7 F/mol, constant current 0.5 A, divided cell;

DOI:10.1021/jo00166a006

upstream raw materials:

methanol

4,4'-dichlorobenzophenone hydrazone

4,4'-Dichlorobenzophenone

bis-(4-chlorophenyl)-dichloromethane

Downstream raw materials:

2,2-bis(4-chloro phenyl)-5-methyl-1,3-dioxane-5-carboxylic acid

C₆₉H₉₃Cl₂NO₁₆

C₂₅H₁₇Cl₅O₅

Methyl (2,2-di[4-chlorophenyl]-1,3-benzodioxolan-5-yl)acetate