Ethyl iMidazo[1,5-a]pyridine-8-carboxylate

Base Information

• Chemical Name: Ethyl iMidazo[1,5-a]pyridine-8-carboxylate
• CAS No.: 697739-12-1
• Molecular Formula: C10H10N2O2
• Molecular Weight: 190.19900
• Hs Code.: 2933990090
• Mol file: 697739-12-1.mol

Synonyms:ethyl imidazol[1,5-a]pyridine-8-carboxylate;

Chemical Property of Ethyl iMidazo[1,5-a]pyridine-8-carboxylate

Chemical Property:

• PSA: 43.60000
• LogP: 1.51100
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

Ethylimidazo[1,5-a]pyridine-8-carboxylate 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Ethyl iMidazo[1,5-a]pyridine-8-carboxylate

There total 6 articles about Ethyl iMidazo[1,5-a]pyridine-8-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

formic acid (64-18-6) + ethyl 2-(aminomethyl)-3-pyridinecarboxylate hydrochloride (697739-11-0) + acetic anhydride (108-24-7) → ethyl imidazo[1,5-a]pyridine-8-carboxylate (697739-12-1)

Guidance literature:

formic acid; acetic anhydride; at 60 ℃; for 2h;

ethyl 2-(aminomethyl)-3-pyridinecarboxylate hydrochloride; at 20 - 35 ℃; for 4h;

Reference yield:

formic acid (64-18-6) + ethyl 2-(aminomethyl)-3-pyridinecarboxylate hydrochloride (697739-11-0) → ethyl imidazo[1,5-a]pyridine-8-carboxylate (697739-12-1)

Guidance literature:

formic acid; With acetic anhydride; at 50 - 60 ℃; for 3h; Inert atmosphere;

ethyl 2-(aminomethyl)-3-pyridinecarboxylate hydrochloride; at 20 ℃; for 8h; Inert atmosphere;

With sodium hydrogencarbonate; In water; Inert atmosphere;

Reference yield:

ethyl 2-(aminomethyl)-3-pyridinecarboxylate hydrochloride (697739-11-0) → ethyl imidazo[1,5-a]pyridine-8-carboxylate (697739-12-1)

Guidance literature:

With acetic anhydride; formyl acetic anhydride; at 20 ℃; for 8h;

upstream raw materials:

formic acid

ethyl 2-(aminomethyl)-3-pyridinecarboxylate hydrochloride

acetic anhydride

3-pyridinecarboxylic acid ethyl ester

Downstream raw materials:

2-(imidazo[1,5-a]pyridin-8-ylmethoxy)-5-methoxybenzaldehyde

imidazo<1,5-a>pyridine-8-carbaldehyde

imidazo[1,5-a]pyridine-8-carboxylic acid

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