2-(PYRIDIN-2-YLAMINOMETHYL)-PHENOL

Base Information

• Chemical Name: 2-(PYRIDIN-2-YLAMINOMETHYL)-PHENOL
• CAS No.: 70301-52-9
• Molecular Formula: C12H12N2O
• Molecular Weight: 200.23600
• Mol file: 70301-52-9.mol

Synonyms:N-(2-pyridyl)-2-oxybenzylamine;2-(pyridin-2-ylamino-methyl)-phenol;2-(o-hydroxybenzylamino)pyridine;N-(2-hydroxybenzyl)-2-aminopyridine;pyridyl-salicylimine;2-(Pyridin-2-ylaminomethyl)-phenol;2-([2]Pyridylamino-methyl)-phenol;

Chemical Property of 2-(PYRIDIN-2-YLAMINOMETHYL)-PHENOL

Chemical Property:

• Melting Point: 105 - 106 °C (methanol)
• PSA: 45.15000
• LogP: 2.47230

Purity/Quality:

99% ^*data from raw suppliers

2-((Pyridin-2-ylamino)methyl)phenol 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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Technology Process of 2-(PYRIDIN-2-YLAMINOMETHYL)-PHENOL

There total 6 articles about 2-(PYRIDIN-2-YLAMINOMETHYL)-PHENOL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

2-aminopyridine (504-29-0) + salicylaldehyde (90-02-8) → 2-<(o-hydroxybenzyl)amino>pyridine (70301-52-9)

Guidance literature:

2-aminopyridine; salicylaldehyde; With sodium sulfate; In dichloromethane; at 20 ℃; for 12h;

With methanol; sodium tetrahydroborate; In dichloromethane; at 20 ℃; for 12h;

DOI:10.1002/ejoc.201900264

Reference yield: 40.0%

2-(pyridine-2-yliminomethyl)phenol (1823-47-8) → 2-<(o-hydroxybenzyl)amino>pyridine (70301-52-9)

Guidance literature:

With sodium cyanoborohydride; In methanol; for 18h; Ambient temperature;

DOI:10.1021/jm00157a020

Reference yield:

2-[(1E)-2-aza-2-(2-pyridyl)ethenyl]benzen-1-ol (17543-97-4) → 2-<(o-hydroxybenzyl)amino>pyridine (70301-52-9)

Guidance literature:

With sodium tetrahydroborate; In methanol; at 0 - 30 ℃;

DOI:10.14233/ajchem.2013.14091

upstream raw materials:

2-(pyridine-2-yliminomethyl)phenol

N-(2'-pyridyl)-2-hydroxybenzamide

2-aminopyridine

salicylaldehyde

Downstream raw materials:

diacetato-bis(N-(2-hydroxybenzyl)-2-aminopyridine)copper(II)

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