Benzamide, 5-bromo-2-iodo-N-methoxy-N-methyl-

Base Information

Chemical Name:Benzamide, 5-bromo-2-iodo-N-methoxy-N-methyl-
CAS No.:842135-31-3
Molecular Formula:C9H9BrINO2
Molecular Weight:369.98200
Hs Code.:

Synonyms:

Suppliers and Price of Benzamide, 5-bromo-2-iodo-N-methoxy-N-methyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Matrix Scientific
5-Bromo-2-iodo-N-methoxy-N-methylbenzamide 95%
5g
$ 1238.00

Total 0 raw suppliers

Chemical Property of Benzamide, 5-bromo-2-iodo-N-methoxy-N-methyl-

Chemical Property:

PSA：29.54000
LogP:2.68710

Purity/Quality:: 5-Bromo-2-iodo-N-methoxy-N-methylbenzamide 95% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Benzamide, 5-bromo-2-iodo-N-methoxy-N-methyl-

There total 1 articles about Benzamide, 5-bromo-2-iodo-N-methoxy-N-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 21740-00-1
5-bromo-2-iodo-benzoic acid

: 6638-79-5
N,O-dimethylhydroxylamine*hydrochloride

: 842135-31-3
5-bromo-2-iodo-N-methoxy-N-methylbenzamide

Guidance literature:: 5-bromo-2-iodo-benzoic acid; With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;

N,O-dimethylhydroxylamine*hydrochloride; With pyridine; In dichloromethane; at 0 - 25 ℃; for 12h;
DOI:10.1021/ol1029035

Reference yield: 34.0%

: 842135-31-3
5-bromo-2-iodo-N-methoxy-N-methylbenzamide

: 536-74-3
phenylacetylene

: 1262282-53-0
N-methoxy-N-methyl-2,5-bis(phenylethynyl)benzamide

Guidance literature:: With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; N-butylamine; In tetrahydrofuran; for 2h; Inert atmosphere;
DOI:10.1021/ol1029035

Reference yield:

: 842135-31-3
5-bromo-2-iodo-N-methoxy-N-methylbenzamide

: 1262282-71-2
(E)-3-[chloro(phenyl)methylene]-6-(phenylethynyl)isobenzofuran-1(3H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; N-butylamine / tetrahydrofuran / 2 h / Inert atmosphere

2: N-chloro-succinimide; copper dichloride / acetonitrile / 100 °C / Inert atmosphere

With N-chloro-succinimide; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; N-butylamine; copper dichloride; In tetrahydrofuran; acetonitrile;
DOI:10.1021/ol1029035