Phosphoric acid, (2S)-2,3-bis(phenylmethoxy)propyl (2R,8R)-8-(hydroxymethyl)-10-(4-methoxyphenyl)-2-[(4-methoxyphenyl) methoxy]-5-oxido-5-(phenylmethoxy)-4,6,9-trioxa-5-phosphadec-1-yl phenylmethyl ester

Base Information

Chemical Name:Phosphoric acid, (2S)-2,3-bis(phenylmethoxy)propyl (2R,8R)-8-(hydroxymethyl)-10-(4-methoxyphenyl)-2-[(4-methoxyphenyl) methoxy]-5-oxido-5-(phenylmethoxy)-4,6,9-trioxa-5-phosphadec-1-yl phenylmethyl ester
CAS No.:849240-72-8
Molecular Formula:C53H62O15P2
Molecular Weight:1001.01
Hs Code.:

Phosphoric acid, (2S)-2,3-bis(phenylmethoxy)propyl
(2R,8R)-8-(hydroxymethyl)-10-(4-methoxyphenyl)-2-[(4-methoxyphenyl)
methoxy]-5-oxido-5-(phenylmethoxy)-4,6,9-trioxa-5-phosphadec-1-yl
phenylmethyl ester

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Phosphoric acid, (2S)-2,3-bis(phenylmethoxy)propyl (2R,8R)-8-(hydroxymethyl)-10-(4-methoxyphenyl)-2-[(4-methoxyphenyl) methoxy]-5-oxido-5-(phenylmethoxy)-4,6,9-trioxa-5-phosphadec-1-yl phenylmethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Phosphoric acid, (2S)-2,3-bis(phenylmethoxy)propyl (2R,8R)-8-(hydroxymethyl)-10-(4-methoxyphenyl)-2-[(4-methoxyphenyl) methoxy]-5-oxido-5-(phenylmethoxy)-4,6,9-trioxa-5-phosphadec-1-yl phenylmethyl ester

There total 9 articles about Phosphoric acid, (2S)-2,3-bis(phenylmethoxy)propyl (2R,8R)-8-(hydroxymethyl)-10-(4-methoxyphenyl)-2-[(4-methoxyphenyl) methoxy]-5-oxido-5-(phenylmethoxy)-4,6,9-trioxa-5-phosphadec-1-yl phenylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 849240-71-7
Phosphoric acid benzyl ester (S)-3-{benzyloxy-[(R)-3-(tert-butyl-diphenyl-silanyloxy)-2-(4-methoxy-benzyloxy)-propoxy]-phosphoryloxy}-2-(4-methoxy-benzyloxy)-propyl ester (S)-2,3-bis-benzyloxy-propyl ester

: 849240-72-8
Phosphoric acid benzyl ester (R)-3-[benzyloxy-((S)-2,3-bis-benzyloxy-propoxy)-phosphoryloxy]-2-(4-methoxy-benzyloxy)-propyl ester (R)-3-hydroxy-2-(4-methoxy-benzyloxy)-propyl ester

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃;
DOI:10.1016/j.tetasy.2004.11.070

Reference yield:

: Phosphorous acid benzyl ester (S)-2,3-bis-benzyloxy-propyl ester (R)-3-(tert-butyl-diphenyl-silanyloxy)-2-(4-methoxy-benzyloxy)-propyl ester

: 849240-72-8
Phosphoric acid benzyl ester (R)-3-[benzyloxy-((S)-2,3-bis-benzyloxy-propoxy)-phosphoryloxy]-2-(4-methoxy-benzyloxy)-propyl ester (R)-3-hydroxy-2-(4-methoxy-benzyloxy)-propyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 3.5 g / tert-butyl hydroperoxide / CH₂Cl₂; decane

2: 87 percent / tetrabutylammonium fluoride / tetrahydrofuran / 20 °C

3: tetrazole / CH₂Cl₂ / 1.5 h / 20 °C

4: 3.1 g / tert-butyl hydroperoxide / CH₂Cl₂; decane

5: 80 percent / tetrabutylammonium fluoride / tetrahydrofuran / 20 °C

With 1H-tetrazole; tert.-butylhydroperoxide; tetrabutyl ammonium fluoride; In tetrahydrofuran; decane; dichloromethane;
DOI:10.1016/j.tetasy.2004.11.070

Reference yield:

: 849240-69-3
benzyl [(2S)-1,2-di-benzyloxy-propan-3-yl] [(2R)-1-tert-butyldiphenylsilyloxy-2-(4-methoxybenzyloxy)propan-3-yl] phosphate

: 849240-72-8
Phosphoric acid benzyl ester (R)-3-[benzyloxy-((S)-2,3-bis-benzyloxy-propoxy)-phosphoryloxy]-2-(4-methoxy-benzyloxy)-propyl ester (R)-3-hydroxy-2-(4-methoxy-benzyloxy)-propyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 87 percent / tetrabutylammonium fluoride / tetrahydrofuran / 20 °C

2: tetrazole / CH₂Cl₂ / 1.5 h / 20 °C

3: 3.1 g / tert-butyl hydroperoxide / CH₂Cl₂; decane

4: 80 percent / tetrabutylammonium fluoride / tetrahydrofuran / 20 °C

With 1H-tetrazole; tert.-butylhydroperoxide; tetrabutyl ammonium fluoride; In tetrahydrofuran; decane; dichloromethane;
DOI:10.1016/j.tetasy.2004.11.070