2,4,6-TRIETHOXYBENZALDEHYDE

Base Information

• Chemical Name: 2,4,6-TRIETHOXYBENZALDEHYDE
• CAS No.: 59652-88-9
• Molecular Formula: C13H18 O4
• Molecular Weight: 238.28
• Hs Code.: 2912499000
• Mol file: 59652-88-9.mol

Synonyms:2,4,6-Triethoxybenzaldehyde;NSC 151974

Chemical Property of 2,4,6-TRIETHOXYBENZALDEHYDE

Chemical Property:

• Vapor Pressure: 7.09E-06mmHg at 25°C
• Melting Point: 98°C
• Boiling Point: 376.8°C at 760 mmHg
• Flash Point: 166.7°C
• PSA: 44.76000
• Density: 1.07g/cm³
• LogP: 2.69520

Purity/Quality:

98%,99%, ^*data from raw suppliers

PhloroglucinolAldehydeTriethylEther ^*data from reagent suppliers

Safty Information:

• Statements: 36/37/38
• Safety Statements: 26-36/37/39

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,4,6-TRIETHOXYBENZALDEHYDE

There total 2 articles about 2,4,6-TRIETHOXYBENZALDEHYDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

ethyl bromide (74-96-4) + 2,4,6-trihydroxybenzaldehyde (487-70-7) → 2,4,6-triethoxy-benzaldehyde (59652-88-9)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 20 - 60 ℃;

Reference yield:

hydrogen cyanide (74-90-8) + 1,3,5-triethoxy benzene (2437-88-9) → 2,4,6-triethoxy-benzaldehyde (59652-88-9)

Guidance literature:

With zinc(II) chloride; benzene; beim Einleiten von HCl in Reaktionsgemisch und Erwaermen mit wss. HCl;

DOI:10.1021/jo01366a003

Reference yield: 92.3%

N-tert-Butylhydroxylamine (16649-50-6) + 2,4,6-triethoxy-benzaldehyde (59652-88-9) → α-(2,4,6-triethoxyphenyl)-N-tert-butylnitrone (223649-91-0)

Guidance literature:

upstream raw materials:

hydrogen cyanide

1,3,5-triethoxy benzene

ethyl bromide

2,4,6-trihydroxybenzaldehyde

Downstream raw materials:

α-(2,4,6-triethoxyphenyl)-N-tert-butylnitrone

(E)-2',6'-dimethoxy-2,4,6-triethoxychalcone

(E)-2,2',4,4',6,6'-hexaethoxychalcone

2,2',4,4',6,6'-hexaethoxychalcone