N-Methyl-N,1,1-triphenylphosphinecarbothioamide

Base Information

Chemical Name:N-Methyl-N,1,1-triphenylphosphinecarbothioamide
CAS No.:87531-20-2
Molecular Formula:C₂₀H₁₈NPS
Molecular Weight:335.409
Hs Code.:
DSSTox Substance ID:DTXSID401241192

Synonyms:N-Methyl-N,1,1-triphenylphosphinecarbothioamide;DTXSID401241192;87531-20-2

Suppliers and Price of N-Methyl-N,1,1-triphenylphosphinecarbothioamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-Methyl-N,1,1-triphenylphosphinecarbothioamide

Chemical Property:

XLogP3:5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:4
Exact Mass:335.08975775
Heavy Atom Count:23
Complexity:350

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CN(C1=CC=CC=C1)C(=S)P(C2=CC=CC=C2)C3=CC=CC=C3

Technology Process of N-Methyl-N,1,1-triphenylphosphinecarbothioamide

There total 1 articles about N-Methyl-N,1,1-triphenylphosphinecarbothioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 19009-45-1
N-methyl-N-phenylthiocarbamoyl chloride

: 65567-06-8,4541-02-0
lithium diphenylphosphide

: 87531-20-2
1-(Diphenylphosphino)-N-methyl-N-phenylthioformamid

Guidance literature:: In tetrahydrofuran; for 14h; Ambient temperature;

Reference yield: 63.0%

: 14879-42-6
iodo(pentacarbonyl)manganese(I)

: 87531-20-2
1-(Diphenylphosphino)-N-methyl-N-phenylthioformamid

: (CO)3MnI((C₆H₅)2PC(S)N(CH₃)(C₆H₅))

Guidance literature:: In tetrahydrofuran; byproducts: CO; under N2, equimolar amts., stirring for 2.5 - 5 h, at 60 - 65°C, removal of solvent; recrystn. from CH2Cl2, washing with n-hexane, elem. anal.;
DOI:10.1016/0022-328X(84)80256-9

Reference yield: 62.0%

: 14100-30-2
pentacarbonylchloromanganese(I)

: 87531-20-2
1-(Diphenylphosphino)-N-methyl-N-phenylthioformamid

: (CO)3Mn(Cl)((C₆H₅)2PC(S)N(CH₃)(C₆H₅))

Guidance literature:: In tetrahydrofuran; byproducts: CO; under N2, equimolar amts., stirring for 2 - 3 h, at 40°C, removal of solvent; recrystn. from CH2Cl2, washing with n-hexane, elem. anal.;
DOI:10.1016/0022-328X(84)80256-9