beta-D-Glucopyranose, 1-deoxy-1-(phenyldithio)-, tetraacetate

Base Information

Chemical Name:beta-D-Glucopyranose, 1-deoxy-1-(phenyldithio)-, tetraacetate
CAS No.:6612-79-9
Molecular Formula:C20H24O9S2
Molecular Weight:472.537
Hs Code.:
NSC Number:108108
Mol file:6612-79-9.mol

Synonyms:6612-79-9;NSC108108;.beta.-D-Glucopyranose, tetraacetate;NSC-108108

Suppliers and Price of beta-D-Glucopyranose, 1-deoxy-1-(phenyldithio)-, tetraacetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of beta-D-Glucopyranose, 1-deoxy-1-(phenyldithio)-, tetraacetate

Chemical Property:

Vapor Pressure:1.95E-11mmHg at 25°C
Melting Point:117-118 °C(Solv: methanol (67-56-1))
Boiling Point:532.9°Cat760mmHg
Flash Point:256.9°C
PSA：165.03000
Density:1.35g/cm³
LogP:2.51000
XLogP3:3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:11
Rotatable Bond Count:12
Exact Mass:472.08617469
Heavy Atom Count:31
Complexity:651

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)OCC1C(C(C(C(O1)SSC2=CC=CC=C2)OC(=O)C)OC(=O)C)OC(=O)C

Technology Process of beta-D-Glucopyranose, 1-deoxy-1-(phenyldithio)-, tetraacetate

There total 10 articles about beta-D-Glucopyranose, 1-deoxy-1-(phenyldithio)-, tetraacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 19879-84-6
tetraacetyl thioglucose

: 108-98-5
thiophenol

: 6612-79-9
phenyl (2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl) disulfide

Guidance literature:: With diethylazodicarboxylate; In tetrahydrofuran; at 20 ℃; for 3h;
DOI:10.1016/j.tetlet.2007.08.106

Reference yield: 93.0%

: 19879-84-6
tetraacetyl thioglucose

: 17665-58-6
benzenesulfinyl-acetonitrile

: 6612-79-9
phenyl (2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl) disulfide

Guidance literature:: In 1,2-dichloro-ethane; Reflux;
DOI:10.1002/ejoc.200900986

Reference yield: 85.0%

: 882-33-7
diphenyldisulfane

: 572-09-8
2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide

: 6612-79-9
phenyl (2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl) disulfide

Guidance literature:: With carbon disulfide; sodiumsulfide nonahydrate; In N,N-dimethyl-formamide; at 20 ℃; for 0.166667h;
DOI:10.1002/ejoc.202100606