2-(4-Bromoanilino)-4-chlorobenzoic acid

Base Information

Chemical Name:2-(4-Bromoanilino)-4-chlorobenzoic acid
CAS No.:90656-46-5
Molecular Formula:C13H9BrClNO2
Molecular Weight:326.577
Hs Code.:
DSSTox Substance ID:DTXSID80539545
Wikidata:Q82415322

Synonyms:2-(4-Bromoanilino)-4-chlorobenzoic acid;90656-46-5;DTXSID80539545

Suppliers and Price of 2-(4-Bromoanilino)-4-chlorobenzoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(4-Bromoanilino)-4-chlorobenzoic acid

Chemical Property:

XLogP3:6.3
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:324.95052
Heavy Atom Count:18
Complexity:295

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC=C1NC2=C(C=CC(=C2)Cl)C(=O)O)Br

Technology Process of 2-(4-Bromoanilino)-4-chlorobenzoic acid

There total 2 articles about 2-(4-Bromoanilino)-4-chlorobenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 50-84-0
2,4 dichlorobenzoic acid

: 106-40-1
4-bromo-aniline

: 90656-46-5
2-(4-Bromo-phenylamino)-4-chloro-benzoic acid

Guidance literature:: With potassium carbonate; copper; In N,N-dimethyl-formamide; at 140 - 150 ℃; Heating;
DOI:10.1007/BF00770449

Reference yield:

: 936-08-3
2-bromo-4-chlorobenzoic acid

: 106-40-1
4-bromo-aniline

: 90656-46-5
2-(4-Bromo-phenylamino)-4-chloro-benzoic acid

Guidance literature:: With 4-methyl-morpholine; copper(I) oxide; In 1,4-dioxane; at 100 ℃; for 3h; Inert atmosphere;
DOI:10.1021/jo5011697

Reference yield:

: 90656-46-5
2-(4-Bromo-phenylamino)-4-chloro-benzoic acid

: 74-88-4
methyl iodide

: 1621107-07-0
C₁₅H₁₃BrClNO₂

Guidance literature:: 2-(4-Bromo-phenylamino)-4-chloro-benzoic acid; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 ℃; for 0.5h;

methyl iodide; In N,N-dimethyl-formamide; mineral oil; at 20 ℃;
DOI:10.1021/jo5011697