2-(1-Phenylethyl)-1,3-benzoxazole

Base Information

• Chemical Name: 2-(1-Phenylethyl)-1,3-benzoxazole
• CAS No.: 91657-27-1
• Molecular Formula: C15H13NO
• Molecular Weight: 223.274
• DSSTox Substance ID: DTXSID80531201
• Nikkaji Number: J2.946.832J

Synonyms:2-(1-Phenylethyl)-1,3-benzoxazole;91657-27-1;DTXSID80531201

Chemical Property of 2-(1-Phenylethyl)-1,3-benzoxazole

Chemical Property:

• PSA: 26.03000
• LogP: 3.97960
• XLogP3: 4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 2
• Exact Mass: 223.099714038
• Heavy Atom Count: 17
• Complexity: 249

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(C1=CC=CC=C1)C2=NC3=CC=CC=C3O2

Technology Process of 2-(1-Phenylethyl)-1,3-benzoxazole

There total 7 articles about 2-(1-Phenylethyl)-1,3-benzoxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) + benzoxazole (273-53-0,29791-96-6) → 2-(1-phenylethyl)benzo[d]oxazole (91657-27-1)

Guidance literature:

With bis(1,5-cyclooctadiene)nickel⁽⁰⁾; [1,3-bis(2,4,6-trimethylphenyl)imidazol]-2-ylidene; In hexane; at 130 ℃; for 2h; Inert atmosphere;

DOI:10.1002/anie.201001470

Reference yield: 80.0%

benzoxazole (273-53-0,29791-96-6) + acetophenone p-toluenesulfonylhydrazone (4545-21-5) → 2-(1-phenylethyl)benzo[d]oxazole (91657-27-1)

Guidance literature:

With copper(l) iodide; lithium tert-butoxide; In toluene; at 110 ℃; for 1.5h; Inert atmosphere;

DOI:10.1021/ja111249p

Reference yield:

styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) + carbon monoxide (201230-82-2) + 2-amino-phenol (95-55-6) → 2-(β-phenylethyl)benzoxazole (83318-25-6) + 2-(1-phenylethyl)benzo[d]oxazole (91657-27-1)

Guidance literature:

With Ru(2 wt%)/CeO2; In tetrahydrofuran; at 160 ℃; for 6h; under 7500.75 Torr; Sealed tube;

upstream raw materials:

styrene

benzoxazole

acetophenone p-toluenesulfonylhydrazone

acetophenone

Downstream raw materials:

2-(1-phenylethyl)benzo[d]oxazole

(S)-2-(1-phenylethyl)benzo[d]oxazole

hydratropic acid

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 91657-27-1 Benzoxazole, 2-(1-phenylethyl)-

Send

Send

Metric Ton KG G Pound L ML

Send

Send