2-Propyl-1,3-dioxolane

Base Information

• Chemical Name: 2-Propyl-1,3-dioxolane
• CAS No.: 3390-13-4
• Molecular Formula: C6H12O2
• Molecular Weight: 116.16
• European Community (EC) Number: 654-483-3
• NSC Number: 86115
• DSSTox Substance ID: DTXSID00276647
• Nikkaji Number: J132.816F
• Wikidata: Q82007269
• Mol file: 3390-13-4.mol

Synonyms:2-Propyl-1,3-dioxolane;3390-13-4;2-Propyldioxolane;1,3-Dioxolane, 2-propyl-;Butanal, cyclic 1,2-ethanediyl acetal;2-propyl dioxolane;NSC86115;Butanal ethylene acetal;1, 2-propyl-;starbld0009875;Butanal,2-ethanediyl acetal;SCHEMBL26196;DTXSID00276647;NSC 86115;NSC-86115;AKOS006275370

Chemical Property of 2-Propyl-1,3-dioxolane

Chemical Property:

• Vapor Pressure: 10.8mmHg at 25°C
• Boiling Point: 132.5°Cat760mmHg
• Flash Point: 33.8°C
• PSA: 18.46000
• Density: 0.93g/cm³
• LogP: 1.15940
• XLogP3: 1.1
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 2
• Exact Mass: 116.083729621
• Heavy Atom Count: 8
• Complexity: 57.5

Purity/Quality:

99%min ^*data from raw suppliers

2-Propyl-1,3-dioxolane ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCC1OCCO1

Technology Process of 2-Propyl-1,3-dioxolane

There total 4 articles about 2-Propyl-1,3-dioxolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethylene glycol (107-21-1) + butyraldehyde (123-72-8) → 2-propyl-1,3-dioxolane (3390-13-4) + 2-Butoxyethanol (111-76-2,9004-77-7) + butan-1-ol (71-36-3)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; at 140 ℃; for 3h; under 51755.2 Torr; Temperature;

Reference yield:

Tetraethylene glycol (112-60-7) + ethylene glycol (107-21-1) + butyraldehyde (123-72-8) + diethylene glycol (111-46-6) + 2,2'-[1,2-ethanediylbis(oxy)]bisethanol (112-27-6) → 2-propyl-1,3-dioxolane (3390-13-4) + 2-Butoxyethanol (111-76-2,9004-77-7) + Diethylene glycol monobutyl ether (112-34-5,9004-77-7) + triethyleneglycol monobutyl ether (143-22-6,9004-77-7) + tetraethylene glycol monobutyl ether (1559-34-8,9004-77-7) + butan-1-ol (71-36-3)

Guidance literature:

With hydrogen; palladium 10% on activated carbon; at 180 ℃; for 2h; under 51716.2 Torr;

Reference yield:

ethylene glycol (107-21-1) + butyraldehyde (123-72-8) → 2-propyl-1,3-dioxolane (3390-13-4) + 2-Butoxyethanol (111-76-2,9004-77-7) + 1,2-dibutoxyethane (112-48-1,31885-97-9) + butan-1-ol (71-36-3)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; at 160 ℃; for 2h; under 51755.2 Torr;

upstream raw materials:

Tetraethylene glycol

ethylene glycol

butyraldehyde

diethylene glycol

Downstream raw materials:

ethene

butyric acid

butanoic acid methyl ester

2-Buthylidenecyclohexanone

Refernces

• 1、 -. "POLYOL ETHERS AND PROCESS FOR MAKING THEM". Page/Page column 7. . Retrieved 2010/03/31.