2,2,5,5-TETRAMETHYL-4-BENZOYLOXYIMINOCHLOROMETHYL-3-IMIDAZOLINE-1-OXYL

Base Information

• Chemical Name: 2,2,5,5-TETRAMETHYL-4-BENZOYLOXYIMINOCHLOROMETHYL-3-IMIDAZOLINE-1-OXYL
• CAS No.: 134279-78-0
• Molecular Formula: C15H17 Cl N3 O3
• Molecular Weight: 322.77
• Mol file: 134279-78-0.mol

Synonyms:2,2,5,5-TETRAMETHYL-4-BENZOYLOXYIMINOCHLOROMETHYL-3-IMIDAZOLINE-1-OXYL

Chemical Property of 2,2,5,5-TETRAMETHYL-4-BENZOYLOXYIMINOCHLOROMETHYL-3-IMIDAZOLINE-1-OXYL

Chemical Property:

• Vapor Pressure: 2.2E-08mmHg at 25°C
• Boiling Point: 436.3°C at 760 mmHg
• Flash Point: 217.7°C
• Density: 1.27g/cm³

Purity/Quality:

97% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of 2,2,5,5-TETRAMETHYL-4-BENZOYLOXYIMINOCHLOROMETHYL-3-IMIDAZOLINE-1-OXYL

There total 3 articles about 2,2,5,5-TETRAMETHYL-4-BENZOYLOXYIMINOCHLOROMETHYL-3-IMIDAZOLINE-1-OXYL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

2,2,5,5-tetramethyl-4-nitromethyleneimidazolidine-1-oxyl (60829-54-1) + benzoyl chloride (98-88-4) → C15H17ClN3O3 (134279-78-0)

Guidance literature:

With triethylamine; In chloroform; at 0 ℃; for 0.25h; Mechanism; other acid chlorides;

DOI:10.1007/BF00965436

Reference yield: 15.0%

2,2,5,5-tetramethyl-4-nitromethyleneimidazolidine-1-oxyl (60829-54-1) + methyl vinyl ketone (78-94-4,25038-87-3) → 4-(5-acetyl-4,5-dihydroisoxazolyl-3)-2,2,5,5-tetramethyl-3-imidazolin-1-oxyl (134279-77-9) + C15H17ClN3O3 (134279-78-0)

Guidance literature:

With benzoyl chloride; triethylamine; In chloroform; at 0 ℃; for 0.25h;

DOI:10.1007/BF00965436

Reference yield:

benzoyl chloride (98-88-4) + C8H13N3O3(1-)*Na(1+) → C15H17ClN3O3 (134279-78-0)

Guidance literature:

With triethylamine; In tetrahydrofuran; at 20 ℃; for 0.5h;

DOI:10.1007/BF00965436

upstream raw materials:

2,2,5,5-tetramethyl-4-nitromethyleneimidazolidine-1-oxyl

benzoyl chloride

methyl vinyl ketone

Downstream raw materials:

2,2,5,5-tetramethyl-3-imidazolin-1-oxyl-4-O-benzoylhydroximic acid chloride hydrochloride

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