Phenethylamine, N,N-dimethyl-beta-ethyl-

Base Information

• Chemical Name: Phenethylamine, N,N-dimethyl-beta-ethyl-
• CAS No.: 33132-91-1
• Molecular Formula: C12H19N
• Molecular Weight: 177.29
• Hs Code.: 2921499090
• NSC Number: 38492
• Nikkaji Number: J50.044E
• Mol file: 33132-91-1.mol

Synonyms:33132-91-1;Phenethylamine, N,N-dimethyl-beta-ethyl-;N,N-Dimethyl-beta-ethylphenethylamine;NSC 38492;BRN 2087924;NSC38492;Benzeneethanamine, beta-ethyl-N,N-dimethyl-;Benzeneethanamine, .beta.-ethyl-N,N-dimethyl-;SCHEMBL3428926;NSC-38492;Phenethylamine,N-dimethyl-.beta.-ethyl-

Chemical Property of Phenethylamine, N,N-dimethyl-beta-ethyl-

Chemical Property:

• Vapor Pressure: 0.0471mmHg at 25°C
• Boiling Point: 236.5°Cat760mmHg
• Flash Point: 88.3°C
• PSA: 3.24000
• Density: 0.903g/cm³
• LogP: 2.74180
• XLogP3: 2.9
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 4
• Exact Mass: 177.151749610
• Heavy Atom Count: 13
• Complexity: 125

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCC(CN(C)C)C1=CC=CC=C1

Technology Process of Phenethylamine, N,N-dimethyl-beta-ethyl-

There total 6 articles about Phenethylamine, N,N-dimethyl-beta-ethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

α-ethylbenzyldimethyl(trimethylsilylmethyl)ammonium iodide (133302-73-5) → 1-propenylbenzene (873-66-5) + N,N-Dimethyl-2-phenyl-butylamin (33132-91-1) + (Z)-5-propylidene-6-(dimethylamino)methyl-1,3-cyclohexadiene (133302-82-6) + (E)-5-propylidene-6-(dimethylamino)methyl-1,3-cyclohexadiene (133302-77-9)

Guidance literature:

With cesium fluoride; In N,N-dimethyl-formamide; at 10 ℃; for 0.5h; Product distribution;

DOI:10.1055/s-1991-26393

Reference yield:

methyl 2-phenylcyclopropane-1-carboxylate (20030-70-0) + trimethylamine (75-50-3) → methyl 3-(benzyl)propanoate (2046-17-5) + N,N-Dimethyl-2-phenyl-butylamin (33132-91-1)

Guidance literature:

In acetonitrile; for 2h; Yield given. Yields of byproduct given; Irradiation;

DOI:10.1039/c39880001183

Reference yield:

α-ethylbenzyldimethyl(trimethylsilylmethyl)ammonium iodide (133302-73-5) → 1-propenylbenzene (873-66-5) + N,N-Dimethyl-2-phenyl-butylamin (33132-91-1) + 1-propyl-2-dimethylaminomethylbenzene (133302-85-9)

Guidance literature:

With potassium hydroxide; cesium fluoride; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; 1.) DMF, 10 deg C, 0,5 h, 2.) EtOH, 60 deg C, 24 h;

DOI:10.1055/s-1991-26393

upstream raw materials:

N,N-Dimethyl-2-phenylbutyramid

α-ethylbenzyldimethyl(trimethylsilylmethyl)ammonium iodide

methyl 2-phenylcyclopropane-1-carboxylate

trimethylamine